590 Jasmine Street REZN19-0005 Environmental Assessment Phase 2PHASE II ENVIRONMENTAL SITE ASSESSMENT REPORT
Of
Parcel RE #170891-0000
West 6th Street & Jasmine Street
Atlantic Beach, Duval County, Florida
(PES Project #150204)
Prepared for:
Sessa Properties, LLC
9378 Arlington Expressway, Suite 315
Jacksonville, Florida 32225
Prepared by:
Pfahler Environmental Services, Inc.
1212 Forest Oaks Drive
Neptune Beach, Florida 32266
March 2015
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page i
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY .................................................................................... 1
2.0 INTRODUCTION ................................................................................................ 3
2.1 Purpose ...................................................................................................... 3
2.2 Scope of Services ...................................................................................... 3
2.3 Limiting Conditions and Methodologies Used............................................. 4
3.0 PROPERTY BACKGROUND ............................................................................ 5
3.1 Property Location and Description ............................................................. 5
3.2 Physical Setting .......................................................................................... 5
3.3 Current Use and Site Improvements .......................................................... 5
3.4 Adjoining Property Use ............................................................................... 5
4.0 PHASE II ACTIVITIES ....................................................................................... 6
4.1 Scope of Assessment ................................................................................. 6
4.1.1 Supplemental Record Review ......................................................... 6
4.1.2 Chemical Testing Plan ..................................................................... 6
4.1.3 Deviations from the Work Plan ........................................................ 6
4.2 Field Sampling and Methods ...................................................................... 6
4.2.1 Soil Sample Collection and Soil-Vapor Screening ........................... 6
4.2.2 Groundwater Sample Collection ...................................................... 7
4.3 Sample Analyses ........................................................................................ 7
4.3.1 Soil................................................................................................... 7
4.3.2 Groundwater .................................................................................... 7
5.0 EVALUATION AND PRESENTATION OF RESULTS ....................................... 8
5.1 Subsurface Conditions ............................................................................... 8
5.1.1 Geologic Setting .............................................................................. 8
5.1.2 Hydrogeologic Conditions ................................................................ 8
5.2 Field and Analytical Data Results ............................................................... 8
5.2.1 Soil Vapor Screening Results .......................................................... 8
5.2.3 Groundwater .................................................................................... 9
6.0 CONCLUSIONS AND RECOMMENDATIONS ................................................ 10
7.0 CLOSURE ........................................................................................................ 11
8.0 REFERENCES ................................................................................................. 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page ii
Figures
Figure 1 - Property Location Map
Figure 2 - Sampling Location Map
Tables
Table 1 - Soil Vapor Screening Data Summary
Table 2 - Soil Analytical Data Summary
Table 3 - Groundwater Analytical Data Summary
Appendices
APPENDIX A - Soil Boring Logs
APPENDIX B - Analytical Laboratory Report
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 1 of 12
1.0 EXECUTIVE SUMMARY
Sessa Properties, LLC (Client) engaged Pfahler Environmental Services, Inc. (PES) to
conduct a Phase II Environmental Site Assessment (ESA) of Parcel RE #170891-0000
located at the southwestern quadrant of West 6th Street and Jasmine Street in Atlantic
Beach, Duval County, Florida, subsequently referred to in this report as "the property".
The Phase II ESA was competed in general accordance with the American Society of
Testing and Materials (ASTM) Standard Practice for Environmental Site Assessments:
Phase II ESA Process (ASTM Designation: E1903-11) and applicable criteria provided
in Florida Department of Environmental Protection (FDEP) Chapter 62-780, Florida
Administrative Code (FAC).
The purpose of the Phase II ESA is to further evaluate the recognized environmental
conditions (RECs) and Business Environmental Risks (BERs) identified in the previous
Phase I ESA report. The goal is to collect sufficient information to determine the
presence or absence of impacted soil and/or groundwater at the property. The Phase
I ESA report (dated February 8, 2015) prepared by PES identified the following:
REC 1 - The 1943 and 1960 historical aerial photographs show a marsh at the
southern half of the property. The 1970 aerial photograph shows that the
ground surface of the property had been completely reworked and appears to
have included filling in the previously noted marsh. The southern half of the
property may have been impacted by a former old dump reportedly operated by
the City of Atlantic Beach in the 1960s and 1970s at the south and west
adjoining properties. Reportedly solid waste was originally brought onto the
properties to fill in wetlands and low areas followed with some trenching and
above grade trash disposal. The likely presence of unknown buried solid waste
at the property is considered a moderate to high environmental risk.
BER 1 – PES observed used tires and solid waste dumped on the ground surface, and visible evidence of buried solid waste at the southern half of the
property. Removal and proper disposal of the waste would be necessary
before the property is suitable for development.
Scope of Work. The Phase II investigation tasks performed to further evaluate the
subsurface condition of the property included installation of five (5) soil borings and
one groundwater probe well using a Geoprobe 7822DT, collection of soil samples for
field soil-vapor screening and chemical analysis, collection of groundwater sample for
chemical analysis, and evaluation of investigative data and preparation of final report.
Sampling Results. No visible evidence of free product or visibly stained soil was
observed during drilling of the boreholes. Soil samples were collected from the
vadose and water table zones at boring locations SB-1 through SB-5 and field-
screened for volatile organic vapors with an Organic Vapor Analyzer (OVA) to identify
any potential soil contamination and assist with determining the ideal location of the
groundwater sampling point. No positive OVA readings were detected in any of the
soil samples collected from borings, except for concentration of 0.3 ppm at a depth of
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 2 of 12
10.0 feet BLS of boring SB-4. Because of the lack of positive OVA readings in the
soil-vapor screening, the soil sample for chemical analysis was collected from a depth
interval of 2.0-3.0 feet BLS at boring location SB4. Analytical results for soil sample
SB-4 indicated no contaminants of concern (COC) concentrations except for the
following:
• B4 – Methylene Chloride 2 milligrams per kilogram (mg/kg), Dimethyl
phthalate at 0.043 mg/kg, Beryllium at 0.058 mg/kg, Cadmium at 0.14
mg/kg, Chromium at 2.9 mg/kg, Copper at 35 mg/kg, Lead at 5.5 mg/kg,
Nickel at 2.1 mg/kg, Zinc at 35 mg/kg, and Mercury at 0.023 mg/kg.
PES selected boring location SB-3 as the groundwater sampling point. A Geoprobe
direct-push technology rig was used to collect groundwater sample GW -1 from a depth
of 12 feet below land surface (BLS). No visible evidence of free product or suspicious
sheen was observed in the groundwater probe well during sample collection.
Analytical results for groundwater sample GW-1 indicated no COC concentrations
except for the following:
• GW-1 – 1,4-Dichlorobenene at 1.1 micrograms per liter (µg/L), Chlorobenzene
at 6 µg/L, Beryllium at 0.0008 milligrams per liter (mg/L), Chromium at
0.017 mg/L, Lead at 0.011 mg/L, Nickel at 0.0029 mg/L, Silver at
0.0015 mg/L, and Mercury at 0.000063 mg/L.
Conclusions. Based on the findings of this investigation, PES’s conclusions are as
follows: - Results of the soil-vapor screening indicated no evidence of soil contamination
in the vadose and water table zones at the boring locations of this investigation.
In addition, although the analytical results indicated detectable COC
concentrations in soil boring SB-4, none of the concentrations are above the
SCTLs provided in FDEP Chapter 62-777, FAC.
- Although the analytical results of the chemical analysis indicated detectable
COC concentrations in groundwater sample GW-1, none of the concentrations
exceed the GCTLs provided in FDEP Chapter 62-777, FAC.
In our opinion, this Phase II ESA has adequately addressed the REC and BER that
were the subject of this investigation, and that further site assessment of the
subsurface soil and groundwater quality is not warranted for the property at this time.
With regards to the buried solid waste identified at the property, further action that
most likely would involve the removal and off-site disposal of the waste material, and
replacement with clean soil should be considered to assure there is a ground surface
suitable for building construction.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 3 of 12
2.0 INTRODUCTION
Sessa Properties, LLC (Client) engaged Pfahler Environmental Services, Inc. (PES)
to conduct a Phase II Environmental Site Assessment (ESA) of Parcel RE #170891-
0000 located at the southwestern quadrant of West 6th Street and Jasmine Street in
Atlantic Beach, Duval County, Florida, subsequently referred to in this report as "the
property". The Phase II assessment was completed in general accordance with the
American Society of Testing and Materials (ASTM) Standard Practice for
Environmental Site Assessments: Phase II ESA Process (ASTM Designation: E1903-
11) and applicable criteria provided in Florida Department of Environmental Protection
(FDEP) Chapter 62-780, Florida Administrative Code (FAC). This report summarizes
the field activities and findings of our investigation.
2.1 Purpose
The purpose of the Phase II ESA is to further evaluate the recognized environmental
conditions (RECs) and Business Environmental Risks (BERs) identified in the previous
Phase I ESA report. The goal is to collect sufficient information to determine the
presence or absence of impacted soil and/or groundwater at the property. The Phase
I ESA report (dated February 8, 2015) prepared by PES identified the following:
REC 1 - The 1943 and 1960 historical aerial photographs show a marsh at the
southern half of the property. The 1970 aerial photograph shows that the
ground surface of the property had been completely reworked and appears to
have included filling in the previously noted marsh. The southern half of the
property may have been impacted by a former old dump reportedly operated by
the City of Atlantic Beach in the 1960s and 1970s at the south and west
adjoining properties. Reportedly solid waste was originally brought onto the
properties to fill in wetlands and low areas followed with some trenching and
above grade trash disposal. The likely presence of unknown buried solid waste
at the property is considered a moderate to high environmental risk.
BER 1 – PES observed used tires and solid waste dumped on the ground
surface, and visible evidence of buried solid waste at the southern half of the
property. Removal and proper disposal of the waste would be necessary
before the property is suitable for development.
2.2 Scope of Services
Based on the findings of PES’s Phase I ESA, the Phase II scope of services included
the following tasks:
• Installation of soil borings at select areas of the property
• Field screening of collected soil samples for volatile organic vapors
• Collection and chemical analyses of soil and groundwater samples
• Evaluation of field observations and sampling results
• Evaluation of the investigative data and preparation of final report
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
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2.3 Limiting Conditions and Methodologies Used
No assessment can eliminate all uncertainty. Furthermore, any sample, either surface
or subsurface taken for chemical analysis may or may not represent a larger
population. Professional judgment and interpretation are inherent in the process and
uncertainty is possible. The number of sampling points may be able to reduce the
uncertainty but at the same time increase the cost of the assessment.
Even when a Phase II ESA is executed with an appropriate site-specific standard of
care, certain conditions present especially difficult detection problems. Such
conditions may include, but are not limited to, complex geological settings, the fate and
transport characteristics of certain hazardous substances and petroleum products, the
distribution of existing contamination, physical limitations imposed by the location of
utilities and other man-made objects, and the limitations of assessment technologies.
A Phase II ESA does not generally require an exhaustive assessment of
environmental conditions on a property. There is a point at which the cost and time
required to obtain the information outweighs the usefulness of that information and, in
fact, may be a material detriment to the orderly completion of real estate transactions.
If hazardous substance or petroleum releases are confirmed on a parcel of property,
the extent of further assessment to delineate the release is related to the degree of
uncertainty that is acceptable to the user with respect to the transaction.
Field measurements and analytical data only represent the site conditions at the time
of sample collection. Therefore, the usability of data collected as part of this Phase II
ESA may have a finite usefulness depending on the application and use being made
of the data. An environmental professional should evaluate whether the generated
data are appropriate for any subsequent use beyond the original purpose for which the
data was collected.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
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3.0 PROPERTY BACKGROUND
3.1 Property Location and Description
The property is located at southwestern quadrant of the intersection of West 6th Street
and Jasmine Street, which is situated in Northwest ¼ of the Northwest ¼ of Section
38, Township 2 South, Range 29 East of Atlantic Beach, Duval County, Florida. The
property location is shown on Figure 1.
According to the Duval County Property Appraiser (DCPA) records, property details
are as follows: • Owner: Hancock Bank
• RE #: 170891-0000
• Property Use: Vacant Residential (0.515 acres) and Jurisdictional Wetlands
(0.11 acres)
• Zoning: ARS-2 (Residential Single Atlantic Beach)
• Land Units: 0.625 acres
3.2 Physical Setting
Topography at the property ranges between 5 feet and 10 feet National Geodetic
Vertical Datum (NGVD). On inspection, the property was observed to be relatively flat
with some undulations (particularly in the southern half) and several areas of subtle
mounding.
Shallow groundwater can be found at a depth of 4 feet below land surface (BLS) or
less and apparently flows in westerly direction towards nearby Intracoastal Waterway.
However, the direction of flow may vary at times due to influence from tidal
fluctuations.
3.3 Current Use and Site Improvements
The property is currently vacant with no identifiable improvements.
3.4 Adjoining Property Use
Adjoining property uses include Residential - single-family beyond 6th Street to the
north; Vacant Residential – auto salvage storage yard to the south; Residential –
single family beyond (unpaved) Jasmine Street to the east; and, Light Industrial – auto
salvage open storage yard to the west.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 6 of 12
4.0 PHASE II ACTIVITIES
4.1 Scope of Assessment
4.1.1 Supplemental Record Review
Aside from our review of the Phase I ESA report prepared by PES, no supplemental
environmental records were reviewed as part of this Phase II ESA.
4.1.2 Chemical Testing Plan
The analytical testing plan was designed to detect the contaminants suspected to be
present in the samples collected. This testing plan included tests which provide quality
assurance (QA) and techniques that provide quality control (QC) over the chemical
analysis. A completed chain of custody record accompanied each sample shipment to
the analytical laboratory. Chain of custody records provide written documentation
regarding sample collection and handling, identify the persons involved in the chain of
sample possession, and a written record of requested analytical parameters.
4.1.3 Deviations from the Work Plan
There were no deviations to the proposed work plan of this Phase II investigation.
4.2 Field Sampling and Methods
PES and Probe Domain (subcontract driller) personnel initiated and completed the
field sampling activities on February 28, 2015. Following the collection of soil and
groundwater samples, all boreholes were backfilled with the soil drill cuttings.
4.2.1 Soil Sample Collection and Soil-Vapor Screening
Probe Domain utilized a Geoprobe 7822DT direct-push technology (DPT) rig to install
five (5) soil borings (- through SB-5) to a depth of 10.0 feet below land surface (BLS)
at the locations shown on Figure 2. The DPT rig hydraulically advanced a 2.25-inch
outside diameter five-foot long carbon steel core barrel equipped with an acrylic inner
sleeve continuously to the required depth at each boring location. The acrylic sleeve
of each core barrel was removed and cut open to expose a 1.125-inch soil core. PES
personnel hand-grabbed soil samples from the cores representing depths 2.0 feet, 4.0
feet, 6.0 feet, and at 10.0 feet BLS, and placed the samples into glass mason jars
(filled to one-half capacity) and sealed the jars with aluminum foil.
Soils collected for chemical analysis were hand-grabbed and placed directly into the
laboratory-supplied containers, except for volatile analysis an Encor (secondary
device) sampler was used to fill the containers. The sample containers were placed
with wet ice in a hard shell cooler and transported along with chain-of-custody to
Advanced Environmental Laboratory (AEL) in Jacksonville.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 7 of 12
4.2.2 Groundwater Sample Collection
Based on the soil-vapor screening results and field observations, PES selected boring
SB-3 as the location to collect the groundwater sample (GW-1). Sample location is
shown on Figure 2. Probe Domain used the Geoprobe to hydraulically advance a 4-
foot long stainless steel screen with 0.006-inch slots that was flush-threaded to carbon
steel push rods to a depth of 12.0 feet BLS. Once the probe well was pushed to the
desired depth, the drill rod was retracted four feet to expose the screen section to the
aquifer. PES personnel then developed the probe well using a peristaltic pump to
remove unwanted sediment and to establish a hydraulic connection with the aquifer.
Following the well development the aquifer was allowed time to stabilize to static
conditions before sample collection. PES personnel used the peristaltic pump to
collect groundwater sample GW -1 by directly filling the laboratory-supplied containers
using the after-pump method. Sample bottles designated for volatile organics analysis
were filled first followed with filling the containers for semi-volatile organics and metals
analyses.
4.3 Sample Analyses
4.3.1 Soil
Soil-Vapor Screening. The soil samples were allowed to equilibrate to the ambient air
temperature before being field-screened using a MiniRAE 3000 Organic Vapor
Analyzer (OVA), equipped with a photo ionization detector (PID). A total of 20 soil
samples were field-screened with the OVA to determine the presence or absence of
volatile organic vapors in the vadose (unsaturated) and water table (saturated) zones.
The screening process involved piercing the aluminum foil seal of a mason jar with the
OVA probe and obtaining a vapor aliquot from the jar’s headspace. The OVA provided
a direct reading of the vapor concentration in parts per million (ppm).
Chemical Analysis. Since no positive OVA readings were detected in the soil
samples, PES selected soil boring SB-4 for chemical analysis based on field
observations. Requested analysis included Priority Pollutant Volatile Organics
(PPVOs) using EPA Method 8260B, Priority Pollutant Semi-Volatile Organics
(PPSVOs) using EPA Method 8270-SIM, and Priority Pollutant Metals using EPA
Methods 6010 and 7470.
4.3.2 Groundwater
The sample containers were placed with wet ice in a hard shell cooler and transported
along with chain-of-custody to AEL. Requested analyses of groundwater sample GW -
1 included PPVOs using EPA Method 8260B, PPSVOs using EPA Method 8270-SIM,
and Priority Pollutant Metals using EPA Methods 6010 and 7470.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 8 of 12
5.0 EVALUATION AND PRESENTATION OF RESULTS
5.1 Subsurface Conditions
5.1.1 Geologic Setting
As described through observation of the soil cores, the site-specific lithology consists
of 4-5 feet of loose orangish brown-brown-grayish brown-light brown sand (fill) with a
2-foot layer of brown-dark brown silty sand at boring SB-3. Followed by 2.5-4 feet of
buried solid waste at the borings, except for boring SB-1 where only a thin (1-2 inches)
lens of debris was encountered at a depth of 4.5-5 feet BLS. A one foot layer of black
sandy silt (muck) was encountered at a depth of 7.0 feet BLS at boring SB-4. These
layers are underlain by either light brown-gray sand or light gray-gray sandy clayey silt
to the end of the borings except for boring SB-1 where brown-gray and dark brown
silty sand was encountered from 7.5 feet BLS to the end of boring.
Solid waste observed soil cores collected from the soil borings (SB-1 through S-5)
consisted of domestic trash, such as paper, plastic, Styrofoam, and glass and wood
which was observed in soil samples collected borings SB-3 and SB-4. Only a thin lens
(1-2 inches) of trash was observed at a depth of 4.5-5 feet BLS of boring SB-1. Based
on the soil cores and our field observations, the buried solid waste appears to be
located in the southern two-thirds of the property. Lithologic descriptions are included
in the soil boring logs provided in Appendix A.
5.1.2 Hydrogeologic Conditions
No surface water features were identified at the property or adjoining properties,
except for drainage ditches along the southern and western boundaries. Surface
water features found in the surrounding area include a tidal marsh approximately 100
feet southeast, two retention ponds 575 feet south, Intracoastal Waterway less than
1,000 feet west and Hopkins Creek approximately 2800 feet east of the property.
Groundwater was encountered in the soil borings at depths between 3.0 feet and 3.5
feet BLS.
5.2 Field and Analytical Data Results
5.2.1 Soil Vapor Screening Results
No visible evidence of free product or visibly stained soil was observed during drilling
of the boreholes. Soil samples were collected from the vadose and water table zones
at boring locations SB-1 through SB-5. The samples were field-screened for volatile
organic vapors with the OVA to identify any potential soil contamination and assist with
determining the ideal location of the groundwater sampling point. No positive OVA
readings were detected in any of the soil samples collected from borings, except for
concentration of 0.3 ppm at a depth of 10.0 feet BLS of boring SB-4. Soil sampling
depths and OVA readings are presented in Table 1 and on the boring logs provided in
Appendix A.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 9 of 12
5.2.2 Soil Analytical Results
Because of the lack of positive OVA readings in the soil-vapor screening, the soil
sample for chemical analysis was collected from a depth interval of 2.0-3.0 feet BLS at
boring location SB4. The sample was submitted to AEL for chemical analysis.
Analytical results for soil sample SB-4 indicated no contaminants of concern (COC)
concentrations except for the following:
• B4 – Methylene Chloride 2 milligrams per kilogram (mg/kg), Dimethyl
phthalate at 0.043 mg/kg, Beryllium at 0.058 mg/kg, Cadmium at 0.14
mg/kg, Chromium at 2.9 mg/kg, Copper at 35 mg/kg, Lead at 5.5 mg/kg,
Nickel at 2.1 mg/kg, Zinc at 35 mg/kg, and Mercury at 0.023 mg/kg.
Soil analytical results along with the applicable FDEP Soil Cleanup Target Levels
(SCTLs) are summarized in Tables 2, 3 and 4. The analytical laboratory report is
provided as Appendix B.
5.2.3 Groundwater
No visible evidence of free product or suspicious sheen was observed in the
groundwater probe well (GW -1) during sample collection. Analytical results for
groundwater sample GW-1 indicated no COC concentrations except for the following:
• GW-1 – 1,4-Dichlorobenene at 1.1 micrograms per liter (µg/L), Chlorobenzene
at 6 µg/L, Beryllium at 0.0008 milligrams per liter (mg/L), Chromium at
0.017 mg/L, Lead at 0.011 mg/L, Nickel at 0.0029 mg/L, Silver at
0.0015 mg/L, and Mercury at 0.000063 mg/L.
The groundwater analytical results along with the applicable FDEP Groundwater
Cleanup Target Levels (GCTLs) are summarized in Tables 5, 6 and 7. The analytical
laboratory report is provided as Appendix B.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 10 of 12
6.0 CONCLUSIONS AND RECOMMENDATIONS
This Phase II ESA was completed in general accordance with environmental
methodologies referred to in ASTM Practice E1903-11 and applicable site assessment
criteria provided in FDEP Chapter 62-780, FAC, and contains all of the limitations
inherent in these methodologies. No other warranties, expressed or implied, are made
as to the professional services provided under the terms of our contract and included
in this report. Based on the findings of this investigation, PES’s conclusions are as
follows:
Soil. Results of the soil-vapor screening indicated no evidence of soil
contamination in the vadose and water table zones at the boring locations of
this investigation. In addition, although the analytical results indicated
detectable COC concentrations in soil boring SB-4, none of the concentrations
are above the SCTLs provided in FDEP Chapter 62-777, FAC.
Groundwater. Although the analytical results of the chemical analysis indicated
detectable COC concentrations in groundwater sample GW -1, none of the
concentrations are above the GCTLs provided in FDEP Chapter 62-777, FAC.
In our opinion, this Phase II ESA has adequately addressed the REC and BER that
were the subject of this investigation, and that further site assessment of the
subsurface soil and groundwater quality is not warranted for the property at this time.
With regards to the buried solid waste identified at the property, further action that
most likely would involve the removal and off-site disposal of the waste material, and
replacement with clean soil should be considered to assure there is a ground surface
suitable for building construction.
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 11 of 12
7.0 CLOSURE
This report has been prepared for the sole benefit of Sessa Properties, LLC, and their
successors and assigns. The report may not be relied upon by any other person or
entity without the express written consent of PES.
Respectfully submitted,
PFAHLER ENVIRONMENTAL SERVICES, INC.
Randall F. Pfahler, PG #1362
Principal Consultant
Date: March 10, 2015
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Page 12 of 12
8.0 REFERENCES
The following references may have been used in the preparation of this report.
• ASTM Standard D 5730 Guide to Site Characteristics for Environmental
Purposes With Emphasis on Soil, Rock, The Vadose Zone and Ground Water
• ASTM Standard E 1903-11 Standard Practice for Environmental Site
Assessments: Phase II Environmental Site Assessment Process
• FDEP Contaminant Cleanup Target Levels – Chapter 62-777, FAC
• FDEP Contaminated Site Cleanup Criteria – Chapter 62-780, FAC
PROJECT NO.:DRAWN BY:
DATE:SCALE:
PROPERTY
N
150205
PROPERTY LOCATION MAP
3/3/15 1” = 2000 FEET
SOURCE: U.S. Geological Survey, Jacksonville Beach Quadrangle Map, Florida (1964, photo revised 1992).
PFAHLER ENVIRONMENTAL
SERVICES, INC.
1212 Forest Oaks Drive
Neptune Beach, Florida 32266
PARCEL RE #170891-0000
West 6th Street and Jasmine Street
Atlantic Beach, Florida
*
Figure 1
PROJECT NO.:DRAWN BY:
DATE:SCALE:
150205
SAMPLING LOCATION MAP
3/6/15 NOT TO SCALE
PFAHLER ENVIRONMENTAL
SERVICES, INC.
1212 Forest Oaks Drive
Neptune Beach, Florida 32266
PARCEL RE #170891-0000
West 6th Street and Jasmine Street
Atlantic Beach, Florida
Figure 2
PROPERTY LINE
WEST 6TH STREET
JASMINE STREET (unpaved)CULVERTDRAINAGE DITCHDRAINAGE DITCHSB-1
SB-2
GW-1
SB-3
SB-4
SB-5
LEGEND
Approximate Location of Soil Boring/Sample
Approximate Location of Groundwater Sample/Soil Boring
NOT TO SCALE
T E L
MA IIMXORP IPAT OF BURIE
D SOLI
D WASTESOLID WASTE BURIED
APPROXIMATELY 5-8 FEET BLS
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Preapproval Program -- Site Assessment
Reporting
150204_Hancock Bank Proprerty_Tables Page 1 of 7
TABLE 1: Soil-Vapor Screening Data Summary
Atlantic Beach, Duval County, FL
BORING DATE DEPTH TO SAMPLE OVA
NO.COLLECTED WATER DEPTH READING COMMENTS
(fbls)(fbls)(ppm)
2.0 0
4.0 0
6.0 0
10.0 0
2.0 0
4.0 0
6.0 0
10.0 0
2.0 0
4.0 0
6.0 0
10.0 0.3
2.0 0 Lab Sample
4.0 0
6.0 0
10.0 0
2.0 0
4.0 0
6.0 0
10.0 0
ppm = parts per million
fbls = feet below land surface
OVA = organic vapor analyzer
NM = mot measured
Site Name: Parcel RE #170891-0000
Site Address: West 6th and Jasmine Streets
SOIL VAPOR SCREENING RESULTSSAMPLE
SB-5 3.02/28/15
SB-4 2/28/15
SB-3 2/28/15
2/28/15 3.5
SB-1 2/28/15 3.5
3.0
3.5
SB-2
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Preapproval Program -- Site Assessment
150204_Hancock Bank Proprerty_Tables Page 2 of 7
TABLE 2: Soil Priority Pollutant Volatile Organics (PPVOs) Analytical Data Summary
Atlantic Beach, Duval County, FL
SB-4 2/28/15 3.0 2.0-3.0 0 0.0012 U 0.0014 U 0.0011 U 0.0038 U 0.0012 U 0.0015 U 0.0012 U 0.001 U 0.0012 U 2 (i)NCD
0.007 0.5 0.6 0.2 2.2 0.09 0.03 0.03 0.007 0.09 340
1.7 60,000 9,200 700 9.9 24,000 18 9.3 0.8 24,000 2,700
1.2 7,500 1,500 130 6.4 4,400 8.8 6.4 0.2 4,400 460
Notes: SCTL = Soil Cleanup Target Level
mg/kg = milligrams per kilogram
LBGC = Leachability Based on Groundwater Criteria specified in Table II of Chapter 62-777, FAC.
DER = Direct Exposure Residential as specified in Table II of Chapter 62-777, FAC.
DEC = Direct Exposure Commercial as specified in Table II of Chapter 62-777, FAC.
ppm = parts per million
OVA = organic vapor analyzer
U = result is below method detection limit
If analyte not detected, method reporting limit is reported in italics (i.e 0.016 U).
Tetra-
Choloro-
ethylene
(mg/kg)
Trichloro-
ethene
(mg/kg)
Vinyl
Chloride
(mg/kg)
1,4-
Dichloro-
benzene
(mg/kg)
Methylene
Chloride
(mg/kg)
Sample
Depth
(fbls)
OVA
(ppm)
Benzene
(mg/kg)
Depth
to
Water
(fbls)
SAMPLE
Toluene
(mg/kg)
Ethyl-
benzene
(mg/kg)
Total
Xylenes
(mg/kg)
Chloro-
benzene
(mg/kg)
Other
PPVOs
(mg/kg)
SCTLS
LBGC
DEC
DER
Site Name: Parcel RE # 170891-0000
Site Address: West 6th and Jasmine Streets
PARAMETERS
Boring/
Label
Date
Collected
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Preapproval Program -- Site Assessment
150204_Hancock Bank Proprerty_Tables Page 3 of 7
Atlantic Beach, Duval County, FL
SB-4 2/28/15 3.0 2.0-3.0 0 0.019 U 0.015 U 0.017 U 0.017 U 0.018 U 0.016 U 0.015 U 0.02 U 0.017 U 0.019 U 0.043 (i)0.024 U 0.018 U NCD
2.1 27 2,500 0.8 8 2.4 0.05 24 77 1,200 380 3,600 1.2 DL
20,000 20,000 300,000 #0.7 #220,000 ##59,000 *390 300 DL
2,400 1,800 21,000 #0.1 #500 ##3,200 690,000 72 55 DL
Notes: SCTLs = Soil Cleanup Target Levels
mg/kg = milligrams per kilogram
LBGC = Leachability Based on Groundwater Criteria specified in Table II of FDEP's Chapter 62-777, FAC.
DER = Direct Exposure Residential as specified in Table II of FDEP's Chapter 62-777, FAC.
DEC = Direct Exposure Commercial as specified in Table II of FDEP's Chapter 62-777, FAC.
ppm = parts per million
OVA = organic vapor analyzer
DL = detection limit
NCD = no concentration detected
(i) = The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
U = result is below method detection limit
* = contamination is not a concern for this expopsure scenario.
# = Site concentration must be converted to Benzo(a)pyrene equivalent before comparison with the appropriate direct exposure SCTL for Benzo(a)pyrene.
If analyte not detected, method reporting limit is reported in italics (i.e 0.016 U).
Site Name: Parcel RE # 170891-0000
Fluoran-
thene
(mg/kg)
Chry-
sene
(mg/kg)
Anthra-
cene
(mg/kg)
Sample
Depth
(fbls)
TABLE 3: Soil Priority Pollutant Semi-Volatile Organics (PPVOs) Analytical Data Summary
Other
PPSVOs
(mg/kg)
Benzo
[b]fluor-
anthene
(mg/kg)
Naph-
thalene
(mg/kg)
Benzo[a]
pyrene
(mg/kg)
SAMPLE
Benzo
[k]fluor-
anthene
(mg/kg)
Site Address: West 6th and Jasmine Streets
Date
Collected
OVA
(ppm)Label
Depth
to
Water
(fbls)
PARAMETERS
Benzo[a]
anthra-
cene
(mg/kg)
Ace-
naph-
thene
(mg/kg)
Ace-
naph-
thylene
(mg/kg)
Dimethyl
phthalate
(mg/kg)
Phenol
(mg/kg)
Bis(2-Ethyl-
hexyl)
phthalate
(mg/kg)
LBGC
SCTLS DEC
DER
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Site Assessment
150204_Hancock Bank Proprerty_Tables Page 4 of 7
Site Address: West 6th and Jasmine Streets
Atlantic Beach, Duval County, Florida
TABLE 4: Groundwater Inorganic (Metals) Analytical Data Summary
Site Name: Parcel RE #170891-000
PARAMETERSSAMPLE
Label Date
Collected
Depth
to Water
(fbls)
Sample
Depth
(fbls)
OVA
(ppm)Antimony (mg/kg)Arsenic (mg/kg)Beryllium (mg/kg)Cadmium (mg/kg)Chromium (mg/kg)Copper (mg/kg)Lead (mg/kg)Nickel (mg/kg)Selenium (mg/kg)Silver (mg/kg)Thallium (mg/kg)Zinc (mg/kg)Mercury (mg/kg)SB-4 2/28/15 3.0 2.0-3.0 0 0.14 U 0.26 U 0.058 0.14 (i)2.9 35 5.5 2.1 0.21 U 0.034 U 0.15 U 35 0.023
5.4 ***63 7.5 38 ******130 5.2 17 2.8 ***2.1
370 12 1,400 1,700 470 89,000 1,400 35,000 11,000 8,200 150 630,000 17
27 2.1 120 82 210 150 400 340 440 410 6.1 26,000 3
Notes:
mg/kg = milligrams per kilogram
LBGC = Leachability Based on Groundwater Criteria specified in Table II of FDEP's Chapter 62-777, FAC.
DER = Direct Exposure Residential as specified in Table II of FDEP's Chapter 62-777, FAC.
DEC = Direct Exposure Commercial as specified in Table II of FDEP's Chapter 62-777, FAC.
ppm = parts per million
OVA = organic vapor analyzer
U = result is below method detection limit
(i) = The re
*** = Leachability values may be derived using TCLP Test to calculate site-specific CTLs.
If analyte not detected, method reporting limit is reported in italics (i.e 0.016 U).
SCTLS
LBGC
DEC
DER
SCTLs = Soil Cleanup Target Levels
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Preapproval Program -- Site Assessment Reporting
150204_Hancock Bank Proprerty_Tables Page 5 of 7
TABLE 5 : Groundwater Priority Pollutant Volatile Organics (PPVOs) Analytical Data Summary
Atlantic Beach, Duval County, FL
Well/ Label Date
Collected
Benzene
(ug/L)
Toluene
(ug/L)
Ethyl
benzene
(ug/L)
Total
Xylenes
(ug/L)
1,4-
Dichloro-
benzene
(ug/L)
Chloro-
benzene
(ug/L)
Tetra-
Choloro-
ethylene
(ug/L)
Trichloro-
ethene
(ug/L)
Vinyl
Chloride
(ug/L)
Methylene
Chloride
(ug/L)
Other
PPVOs
(ug/L)
GW-1 2/28/15 0.21 U 0.23 U 0.24 U 0.53 U 1.1 6 0.36 U 0.29 U 0.24 U 1 U NCD
1 40 30 20 75 100 3 3 1 5 DL
100 400 300 200 750 1,000 300 300 100 500 DL
Notes: ug/L = micrograms per liter
GCTLs = Groundwater Cleanup Target Levels specified in Chapters 62-550, FAC and 62-777, FAC.
NADCs = Natural Attenuation Default Concentrations specified in Table V of Chapter 62-777, FAC.
VOHs = Volatile Organic Halocarbons
DL = detection limit
(i) = The reported value is between the laboratory method detection limit and the practical quantitation limit.
U = result is below method detection limit
NCD = no concentration detected
If analyte not detected, method reporting limit is reported in italics (i.e 0.021 U).
GCTLs
NADCs
Site Name: Parcel RE # 170891-0000
Site Address: West 6th and Jasmine Streets
SAMPLE PARAMETERS
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Preapproval Program -- Site Assessment Reporting
150204_Hancock Bank Proprerty_Tables Page 6 of 7
Atlantic Beach, Duval County, FL
Well Date
Collected
Ace-
naph-
thene
(ug/L)
Ace-
naph-
thylene
(ug/L)
Anthra-
cene
(ug/L)
Benzo[a]
anthra-
cene
(ug/L)
Benzo[a]
pyrene
(ug/L)
Benzo
[b]fluor-
anthene
(ug/L)
Phenol
(ug/L)
Benzo
[k]fluor-
anthene
(ug/L)
Chrysene
(ug/L)
Fluor-
anthene
(ug/L)
Dimethyl
phthalate
(ug/L)
Bis(2-
Ethyl-
hexyl)
phthalate
(ug/L)
Naph-
thalene
(ug/L)
Other
PPSVOs
(ug/L)
GW-1 2/28/15 0.96 U 0.84 U 0.5 U 0.54 U 0.58 U 0.77 U 0.54 U 0.7 U 0.67 U 0.85 U 1.4 U 1.4 U 1.2 U NCD
20 210 2100 0.05 0.2 **0.05 10 0.5 4.8 280 70,000 6 14 DL
200 2100 21000 5 20 5 100 50 480 2800 7000,000 60 140 DL
Notes: ug/L = micrograms per liter
GCTLs = Groundwater Cleanup Target Levels specified in Table I of Chapter 62-777, FAC.
NADCs = Natural Attenuation Default Concentrations specified in Table V of Chapter 62-777, FAC.
DL = detection limitr
** = As provided in Chapter 62-550, FAC.
(i) = The reported value is between the laboratory method detection limit and the practical quantitation limit.
U = result is below method detection limit
If analyte not detected, method reporting limit is reported in italics (i.e 0.021 U).
Site Address: West 6th and Jasmine Streets
TABLE 6: Groundwater Priority Pollutant Semi-Volatile Organics (PPSVOs) Analytical Data Summary
SAMPLE
Site Name: Parcel RE # 170891-0000
PARAMETERS
GCTLs
NADCs
Florida Department of Environmental Protection -- Bureau of Petroleum Storage Systems -- Site Assessment
150204_Hancock Bank Proprerty_Tables Page 7 of 7
Site Address: West 6th and Jasmine Streets
Atlantic Beach, Duval County, Florida
Label Date
Collected
Antimony
(mg/L)
Arsenic
(mg/L)
Beryllium
(mg/L)
Cadmium
(mg/L)
Chromium
(mg/L)
Copper
(mg/L)
Lead
(mg/L)
Nickel
(mg/L)
Selenium
(mg/L)
Silver
(mg/L)
Thallium
(mg/L)
Zinc
(mg/L)
Mercury
(mg/L)
GW-1 2/28/15 0.006 U 0.0085 U 0.0008 0.00032 U 0.017 0.0025 U 0.011 0.0029(i)0.0068 U 0.0015(i)0.0055 U 0.035 U 0.000063(i)
0.006 0.05 0.004 0.005 0.1 1 0.015 0.1 0.05 0.1 0.002 5 0.002
0.06 0.5 0.04 0.05 1 10 0.15 1 0.5 1 0.02 50 0.02
Notes: mg/L = milligrams per liter
GCTLs = Groundwater Cleanup Target Levels specified in Table I of Chapter 62-777, FAC.
NADCs = Natural Attenuation Default Concentrations specified in Table V of Chapter 62-777, FAC.
** = As provided in Chapter 62-550, FAC.
(i) = The reported value is between the laboratory method detection limit and the practical quantitation limit.
U = result is below method detection limit
If analyte not detected, method reporting limit is reported in italics (i.e 0.021 U).
Site Name: Parcel RE #170891-0000
Sample
GCTLs
TABLE 7: Groundwater Inorganic (Metals) Analytical Data Summary
NADCS
Parameter Results
APPENDICES
Appendix A
Soil Boring Logs
J-lorida Department ofEnvirorullCIItlll Protcctiun-Divhion of Waste Ma.lagemcnt • 1\orcau of Peuoleum S!oroge Systems
BORING LOG
Pogo l of I
~<;fl:J\ .k " '
' :-15_ r ,M r--;;;;-
PARCEL #170391-0000 EndDaio: End Time; rAM rPM
' ' ' ~NA-R~ I~ · · ' '1n
;;;; '~~~''" ( '
I ~ --" ' ' ' 3!5
[check m<tl-od(>)]: ro~ r Spread R u r ~'tockpilc: r ot~tor
~· ( "
(cit<:ckone)r Well r Grout r B<>lt.<lnite ,, r Oth<.T(describc)
'
Lo;, • ~ ;'[€' • ~ I ' "' l " i'} ~-:!! ~ Sampk Description Samples (ti>! ~ '~ > 00 • • •• -·. ~ ' i .u,-, baoed on (IS!":S, oo.r., ... ioinu, ood •
~ ;;:i' " . -' " "'"pte xo.,t.cr -. • 0 otlo..-"'"" .. ) ' and de-ptb or ,, ' . ' , [ • -. • '
{7
' ~trv
6 '
; I IAi
0 ' ~
6
II ~" ;fit_ Jf
; L~
' -;;; ~· ,, l$'M
• '/~ott~ (') 9.~
" D')', M-MCilSt, W Wot; .'
Florida DcJl"rrmenl ofEnvir<l!llilon!al Protectioo • Division of Waste Manog=t-Bureou ofPotroleum Storage Sy'iemS
BORING LOG
PARCEL #170891-0000
·~ r Grom r &nton~c r Other(dcscribe)
" j~ i r,:;;;;;;;;;;;
;"~ • $ ' 0 " 5'}
, • n ' . ·-a a • Samples (list • • • ;. ~ • ' ji:? [~ ~ ' ' n ,.mpl<......a>eJ· . , ,, > ' • aoddep<h "' ,, , r • •• 0 , r ~ ~· "1; ?fro
11 '
/ }v
II""
Florida l)cpartment of Environmeirtal Protection-Division nfWuste Mmagement-E\!re<O of Petroleum ~torage Systems
f' ,:;
' '
PARCEL 11170891-0000
BORING LOG
,----jR\'ffi'~~-~,.,
Eild Time:
r ~ r '" ("AM rPM
' < one)r Well r Grout r Bmtonite r oth<:r(describeJ
• ~ ~ ~ • -· ! 0 •• !10 q, ~ • p '?l • J ~ • <
' n ' Samples (li<t -~ ,. • 0 •• .. ~ • ,, ' =o ' . ~ • ~ • • ., I 0 ' <l'.S ~§ j! > otlou '"''".,."") ' • • ~· • • • -. ~ ' ' ~ . r; )fHII;Y&"' ¥f ' '
M ' I '
f) '
~I
\
n
Florida Oq>llfllll<llt of£n,ironmcolal Protectum-Division of Waste Management • Bureau of Petroleum Stl>rag;; S)!!llemS
BORING LOG
End TIIIU:;
~'}() ' ' ' ~ I '~Ia
·~~ 3 I
' I);
r Drom r ~-1) ·-·
I . Wcll r Groll\ l B<ntonile r oroo-(d .. cribel
e • ~
' il • • "'" • ' 0 • • •• • • ' ' '
H-r-t-+-+=-h:2'ffi~~~~~··", rl"""'-. /JI
e-+-+---+---+---+'n~· .),0, u ''"
-
hY--~~-4~~/· ~
I
I () c
Flmid• Dep!!rtillC!llof P.twiro!!Ill<Jrllll Prot<ction-Divh1on of Waste Manogti!Ient-B=u of Petroleum Stornge Systaus
BORING LOG ,,, '
~t:fl£
~~;, r.~r-,M
PARCEL 1170891-0000 End Time: r· AM !" PM '.,.,_ ' ..
' R Pfahler
-~ ~ li . ' ,, ' 0 ~I " I ,_;"
'"'~ 3 ' (lj' ' ,,, " '" -,, I ' r _, Sp=d X Bookfill f Stockpli< r Olh<T
' . . :;;;' Wo" r Grout f Be!ttonite fi., Bod::fill r Od= (describe)
" ~ • -· • f :q ' '~ 0 • • -::-. "2. ~ 0 Sample n h-• Samples fful . ' ·-' • • g.= ;. ~ ~ (loc!JK!< gnolo size bo"'d • • 'ii ,;g ' -llllllp!<...,.\o<r •• ""'" ''"""!«) ' ""d doplb 01" ,, < •• 0 • • -. " • '
If', "" 'l 'f_, '
brC ' '
f /() ' "
'
I,,~ 9-JAlq ' :/);, ,,_,_ ~f
(J •
I 'i·! -~ ,. rf1 "' (JJ / t:t~-Ill '
leA. "' !.
' 1(6.; ~ >:) /J -)~r
'-!\ II/ "
: !)-Dr,c ll MoiSl; WmW~~-!-s;;;; ;.,..,, "
Appendix B
Analytical Laboratory Report
Advanced Environmental Laboratories, Inc
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 1 of 20
Randy Pfahler
Pfahler Environmental Services
1212 Forest Oaks Dr
Neptune Beach, FL 32266
March 10, 2015
RE:Workorder:J1501847 Hancock Bank Property
Dear Randy Pfahler:
Enclosed are the analytical results for sample(s) received by the laboratory on Monday, March 02, 2015. Results reported herein conform
to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. The analytical results for the
samples contained in this report were submitted for analysis as outlined by the Chain of Custody and results pertain only to these samples.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Enclosures
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
Advanced Environmental Laboratories, Inc
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 2 of 20
SAMPLE SUMMARY
Workorder:J1501847 Hancock Bank Property
Lab ID Sample ID Matrix Date Collected Date Received
J1501847001 GW-1 Water 2/28/2015 13:45 3/2/2015 08:54
J1501847002 SB-4 Soil 2/28/2015 14:05 3/2/2015 08:54
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
Advanced Environmental Laboratories, Inc
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 3 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
GW-1
Matrix:Water
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847001
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 13:45
Sample Description:Location:
Adjusted
PQL Lab
METALS
Analysis Desc: SW846 6010B
Analysis,Water
Preparation Method: SW-846 3010A
Analytical Method: SW-846 6010
Antimony 0.0060 mg/L 0.0301 3/4/2015 13:41U0.0060 J
Arsenic 0.0085 mg/L 0.0101 3/4/2015 13:41U0.0085 J
Beryllium 0.00080 mg/L 0.000301 3/4/2015 13:410.00013 J
Cadmium 0.00032 mg/L 0.000601 3/4/2015 13:41U0.00032 J
Chromium 0.017 mg/L 0.00101 3/4/2015 13:410.00050 J
Copper 0.0025 mg/L 0.00401 3/4/2015 13:41U0.0025 J
Lead 0.011 mg/L 0.00701 3/4/2015 13:410.0013 J
Nickel 0.0029 mg/L 0.00651 3/4/2015 13:41I0.0011 J
Selenium 0.0068 mg/L 0.0201 3/4/2015 13:41U0.0068 J
Silver 0.0015 mg/L 0.00401 3/4/2015 13:41I0.00044 J
Thallium 0.0055 mg/L 0.0251 3/4/2015 13:41U0.0055 J
Zinc 0.035 mg/L 0.0101 3/4/2015 13:410.0020 J
Analysis Desc: SW846 7470A
Analysis,Water
Preparation Method: SW-846 7470A
Analytical Method: SW-846 7470A
Mercury 0.000063 mg/L 0.000101 3/9/2015 13:29I0.000010 J
SEMIVOLATILES
Analysis Desc: 8270C Analysis, Water Preparation Method: SW-846 3510C
Analytical Method: SW-846 8270C
1,2,4-Trichlorobenzene 0.69 ug/L 5.01 3/6/2015 21:42U0.69 J
1,2-Dichlorobenzene 1.4 ug/L 5.01 3/6/2015 21:42U1.4 J
1,2-Diphenylhydrazine 0.96 ug/L 5.01 3/6/2015 21:42U0.96 J
1,3-Dichlorobenzene 1.0 ug/L 5.01 3/6/2015 21:42U1.0 J
1,4-Dichlorobenzene 1.2 ug/L 5.01 3/6/2015 21:42U1.2 J
2,4,6-Trichlorophenol 0.93 ug/L 5.01 3/6/2015 21:42U0.93 J
2,4-Dichlorophenol 0.90 ug/L 5.01 3/6/2015 21:42U0.90 J
2,4-Dimethylphenol 2.6 ug/L 5.01 3/6/2015 21:42U2.6 J
2,4-Dinitrophenol 0.62 ug/L 101 3/6/2015 21:42U0.62 J
2,4-Dinitrotoluene (2,4-DNT)0.60 ug/L 5.01 3/6/2015 21:42U0.60 J
2,6-Dinitrotoluene (2,6-DNT)1.1 ug/L 5.01 3/6/2015 21:42U1.1 J
2-Chloronaphthalene 0.97 ug/L 5.01 3/6/2015 21:42U0.97 J
2-Chlorophenol 1.2 ug/L 5.01 3/6/2015 21:42U1.2 J
2-Methyl-4,6-dinitrophenol 0.77 ug/L 5.01 3/6/2015 21:42U0.77 J
2-Nitrophenol 0.63 ug/L 5.01 3/6/2015 21:42U0.63 J
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
Advanced Environmental Laboratories, Inc
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 4 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
GW-1
Matrix:Water
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847001
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 13:45
Sample Description:Location:
Adjusted
PQL Lab
3,3`-Dichlorobenzidine 1.3 ug/L 5.01 3/6/2015 21:42U1.3 J
4-Bromophenyl Phenyl Ether 1.1 ug/L 5.01 3/6/2015 21:42U1.1 J
4-Chloro-3-methylphenol 0.62 ug/L 5.01 3/6/2015 21:42U0.62 J
4-Chlorophenyl Phenyl Ether 0.69 ug/L 5.01 3/6/2015 21:42U0.69 J
4-Nitrophenol 0.62 ug/L 5.01 3/6/2015 21:42U0.62 J
Acenaphthene 0.96 ug/L 5.01 3/6/2015 21:42U0.96 J
Acenaphthylene 0.84 ug/L 5.01 3/6/2015 21:42U0.84 J
Anthracene 0.50 ug/L 5.01 3/6/2015 21:42U0.50 J
Benzidine 0.74 ug/L 5.01 3/6/2015 21:42U0.74 J
Benzo[a]anthracene 0.54 ug/L 5.01 3/6/2015 21:42U0.54 J
Benzo[a]pyrene 0.58 ug/L 5.01 3/6/2015 21:42U0.58 J
Benzo[b]fluoranthene 0.77 ug/L 5.01 3/6/2015 21:42U0.77 J
Benzo[g,h,i]perylene 0.76 ug/L 5.01 3/6/2015 21:42U0.76 J
Benzo[k]fluoranthene 0.70 ug/L 5.01 3/6/2015 21:42U0.70 J
Butyl benzyl phthalate 1.1 ug/L 5.01 3/6/2015 21:42U1.1 J
Chrysene 0.67 ug/L 5.01 3/6/2015 21:42U0.67 J
Di-n-Butyl Phthalate 0.88 ug/L 5.01 3/6/2015 21:42U0.88 J
Di-n-octyl Phthalate 1.2 ug/L 5.01 3/6/2015 21:42U1.2 J
Dibenzo[a,h]anthracene 0.73 ug/L 5.01 3/6/2015 21:42U0.73 J
Diethyl phthalate 0.98 ug/L 5.01 3/6/2015 21:42U0.98 J
Dimethyl phthalate 1.4 ug/L 5.01 3/6/2015 21:42U1.4 J
Fluoranthene 0.64 ug/L 5.01 3/6/2015 21:42U0.64 J
Fluorene 0.85 ug/L 5.01 3/6/2015 21:42U0.85 J
Hexachlorobenzene 0.99 ug/L 5.01 3/6/2015 21:42U0.99 J
Hexachlorobutadiene 0.87 ug/L 5.01 3/6/2015 21:42U0.87 J
Hexachlorocyclopentadiene 0.99 ug/L 5.01 3/6/2015 21:42U0.99 J
Hexachloroethane 1.2 ug/L 5.01 3/6/2015 21:42U1.2 J
Indeno(1,2,3-cd)pyrene 0.68 ug/L 5.01 3/6/2015 21:42U0.68 J
Isophorone 1.1 ug/L 5.01 3/6/2015 21:42U1.1 J
N-Nitrosodi-n-propylamine 2.2 ug/L 5.01 3/6/2015 21:42U2.2 J
N-Nitrosodimethylamine 0.62 ug/L 5.01 3/6/2015 21:42U0.62 J
N-Nitrosodiphenylamine 0.59 ug/L 5.01 3/6/2015 21:42U0.59 J
Naphthalene 1.2 ug/L 5.01 3/6/2015 21:42U1.2 J
Nitrobenzene 1.1 ug/L 5.01 3/6/2015 21:42U1.1 J
Pentachlorophenol 0.95 ug/L 5.01 3/6/2015 21:42U0.95 J
Phenanthrene 0.55 ug/L 5.01 3/6/2015 21:42U0.55 J
Phenol 0.54 ug/L 5.01 3/6/2015 21:42U0.54 J
Pyrene 0.59 ug/L 5.01 3/6/2015 21:42U0.59 J
bis(2-Chloroethoxy)methane 1.2 ug/L 5.01 3/6/2015 21:42U1.2 J
bis(2-Chloroethyl)Ether 1.5 ug/L 5.01 3/6/2015 21:42U1.5 J
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 5 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
GW-1
Matrix:Water
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847001
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 13:45
Sample Description:Location:
Adjusted
PQL Lab
bis(2-Chloroisopropyl) Ether 1.4 ug/L 5.01 3/6/2015 21:42U1.4 J
bis(2-Ethylhexyl) phthalate 1.4 ug/L 5.01 3/6/2015 21:42U1.4 J
2-Fluorophenol (S)58 %10-901 3/6/2015 21:42
Phenol-d6 (S)43 %10-671 3/6/2015 21:42
Nitrobenzene-d5 (S)103 %32-1471 3/6/2015 21:42
2-Fluorobiphenyl (S)81 %34-1401 3/6/2015 21:42
2,4,6-Tribromophenol (S)89 %19-1901 3/6/2015 21:42
p-Terphenyl-d14 (S)93 %54-1381 3/6/2015 21:42
VOLATILES
Analysis Desc: 8260B Analysis, Water Preparation Method: SW-846 5030B
Analytical Method: SW-846 8260B
1,1,1-Trichloroethane 0.22 ug/L 1.01 3/3/2015 21:13U0.22 J
1,1,2,2-Tetrachloroethane 0.20 ug/L 1.01 3/3/2015 21:13U0.20 J
1,1,2-Trichloroethane 0.30 ug/L 1.01 3/3/2015 21:13U0.30 J
1,1-Dichloroethane 0.14 ug/L 1.01 3/3/2015 21:13U0.14 J
1,1-Dichloroethylene 0.18 ug/L 1.01 3/3/2015 21:13U0.18 J
1,2-Dichlorobenzene 0.18 ug/L 1.01 3/3/2015 21:13U0.18 J
1,2-Dichloroethane 0.23 ug/L 1.01 3/3/2015 21:13U0.23 J
1,2-Dichloropropane 0.20 ug/L 1.01 3/3/2015 21:13U0.20 J
1,3-Dichlorobenzene 0.19 ug/L 1.01 3/3/2015 21:13U0.19 J
1,4-Dichlorobenzene 1.1 ug/L 1.01 3/3/2015 21:130.22 J
2-Chloroethyl Vinyl Ether 0.20 ug/L 5.01 3/3/2015 21:13U0.20 J
Acrolein (Propenal)1.2 ug/L 5.01 3/3/2015 21:13U1.2 J
Acrylonitrile 1.1 ug/L 5.01 3/3/2015 21:13U1.1 J
Benzene 0.21 ug/L 1.01 3/3/2015 21:13U0.21 J
Bromodichloromethane 0.25 ug/L 1.01 3/3/2015 21:13U0.25 J
Bromoform 0.43 ug/L 5.01 3/3/2015 21:13U0.43 J
Bromomethane 0.24 ug/L 1.01 3/3/2015 21:13U0.24 J
Carbon Tetrachloride 0.36 ug/L 1.01 3/3/2015 21:13U0.36 J
Chlorobenzene 6.0 ug/L 1.01 3/3/2015 21:130.21 J
Chloroethane 0.33 ug/L 1.01 3/3/2015 21:13U0.33 J
Chloroform 0.18 ug/L 1.01 3/3/2015 21:13U0.18 J
Chloromethane 0.21 ug/L 1.01 3/3/2015 21:13U0.21 J
Dibromochloromethane 0.33 ug/L 1.01 3/3/2015 21:13U0.33 J
Dichlorodifluoromethane 0.15 ug/L 1.01 3/3/2015 21:13U0.15 J
Ethylbenzene 0.24 ug/L 1.01 3/3/2015 21:13U0.24 J
Methylene Chloride 1.0 ug/L 5.01 3/3/2015 21:13U1.0 J
Tetrachloroethylene (PCE)0.36 ug/L 1.01 3/3/2015 21:13U0.36 J
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 6 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
GW-1
Matrix:Water
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847001
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 13:45
Sample Description:Location:
Adjusted
PQL Lab
Toluene 0.23 ug/L 1.01 3/3/2015 21:13U0.23 J
Trichloroethene 0.29 ug/L 1.01 3/3/2015 21:13U0.29 J
Trichlorofluoromethane 0.32 ug/L 1.01 3/3/2015 21:13U0.32 J
Vinyl Chloride 0.24 ug/L 1.01 3/3/2015 21:13U0.24 J
Xylene (Total)0.53 ug/L 3.01 3/3/2015 21:13U0.53 J
cis-1,2-Dichloroethylene 0.24 ug/L 1.01 3/3/2015 21:13U0.24 J
cis-1,3-Dichloropropene 0.16 ug/L 1.01 3/3/2015 21:13U0.16 J
trans-1,2-Dichloroethylene 0.20 ug/L 1.01 3/3/2015 21:13U0.20 J
trans-1,3-Dichloropropylene 0.18 ug/L 5.01 3/3/2015 21:13U0.18 J
1,2-Dichloroethane-d4 (S)97 %80-1201 3/3/2015 21:13
Toluene-d8 (S)104 %88-1101 3/3/2015 21:13
Bromofluorobenzene (S)102 %86-1151 3/3/2015 21:13
03/02/15 08:54
SB-4
Matrix:Soil
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847002
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 14:05
Sample Description:Location:
Results for sample J1501847002 are reported on a dry weight basis.
Adjusted
PQL Lab
METALS
Analysis Desc: SW846 6010B
Analysis,Soils
Preparation Method: SW-846 3050B
Analytical Method: SW-846 6010
Antimony 0.14 mg/Kg 0.851 3/5/2015 00:18U0.14 J
Arsenic 0.26 mg/Kg 0.281 3/5/2015 00:18U0.26 J
Beryllium 0.058 mg/Kg 0.00851 3/5/2015 00:180.0024 J
Cadmium 0.14 mg/Kg 0.171 3/5/2015 00:18I0.036 J
Chromium 2.9 mg/Kg 0.111 3/5/2015 00:180.067 J
Copper 35 mg/Kg 0.111 3/5/2015 00:180.061 J
Lead 5.5 mg/Kg 0.201 3/5/2015 00:180.057 J
Nickel 2.1 mg/Kg 0.181 3/5/2015 00:180.055 J
Selenium 0.21 mg/Kg 0.571 3/5/2015 00:18U0.21 J
Silver 0.034 mg/Kg 0.111 3/5/2015 00:18U0.034 J
Thallium 0.15 mg/Kg 0.711 3/5/2015 00:18U0.15 J
Zinc 35 mg/Kg 0.281 3/5/2015 00:180.21 J
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
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Report ID: 357001 - 5175626 Page 7 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
SB-4
Matrix:Soil
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847002
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 14:05
Sample Description:Location:
Results for sample J1501847002 are reported on a dry weight basis.
Adjusted
PQL Lab
Analysis Desc: SW846 7471A Analysis,
Soil
Preparation Method: SW-846 7471A
Analytical Method: SW-846 7471A
Mercury 0.023 mg/Kg 0.00521 3/6/2015 11:340.00073 J
SEMIVOLATILES
Analysis Desc: 8270C Analysis, Soil Preparation Method: SW-846 3550B
Analytical Method: SW-846 8270C
1,2,4-Trichlorobenzene 0.026 mg/Kg 0.201 3/7/2015 04:45U0.026 J
1,2-Dichlorobenzene 0.028 mg/Kg 0.201 3/7/2015 04:45U0.028 J
1,2-Diphenylhydrazine 0.016 mg/Kg 0.201 3/7/2015 04:45U0.016 J
1,3-Dichlorobenzene 0.024 mg/Kg 0.201 3/7/2015 04:45U0.024 J
1,4-Dichlorobenzene 0.030 mg/Kg 0.201 3/7/2015 04:45U0.030 J
2,4,6-Trichlorophenol 0.022 mg/Kg 0.201 3/7/2015 04:45U0.022 J
2,4-Dichlorophenol 0.026 mg/Kg 0.201 3/7/2015 04:45U0.026 J
2,4-Dimethylphenol 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
2,4-Dinitrophenol 0.065 mg/Kg 0.401 3/9/2015 19:31U0.065 J
2,4-Dinitrotoluene (2,4-DNT)0.022 mg/Kg 0.201 3/7/2015 04:45U0.022 J
2,6-Dinitrotoluene (2,6-DNT)0.032 mg/Kg 0.201 3/7/2015 04:45U0.032 J
2-Chloronaphthalene 0.021 mg/Kg 0.201 3/7/2015 04:45U0.021 J
2-Chlorophenol 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
2-Methyl-4,6-dinitrophenol 0.044 mg/Kg 0.201 3/7/2015 04:45U0.044 J
2-Nitrophenol 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
3,3`-Dichlorobenzidine 0.030 mg/Kg 0.201 3/7/2015 04:45U0.030 J
4-Bromophenyl Phenyl Ether 0.027 mg/Kg 0.201 3/7/2015 04:45U0.027 J
4-Chloro-3-methylphenol 0.016 mg/Kg 0.201 3/7/2015 04:45U0.016 J
4-Chlorophenyl Phenyl Ether 0.030 mg/Kg 0.201 3/7/2015 04:45U0.030 J
4-Nitrophenol 0.049 mg/Kg 0.201 3/7/2015 04:45U0.049 J
Acenaphthene 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
Acenaphthylene 0.015 mg/Kg 0.201 3/7/2015 04:45U0.015 J
Anthracene 0.017 mg/Kg 0.201 3/7/2015 04:45U0.017 J
Benzidine 0.014 mg/Kg 0.201 3/7/2015 04:45U0.014 J
Benzo[a]anthracene 0.017 mg/Kg 0.201 3/7/2015 04:45U0.017 J
Benzo[a]pyrene 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
Benzo[b]fluoranthene 0.016 mg/Kg 0.201 3/7/2015 04:45U0.016 J
Benzo[g,h,i]perylene 0.022 mg/Kg 0.201 3/7/2015 04:45U0.022 J
Benzo[k]fluoranthene 0.020 mg/Kg 0.201 3/7/2015 04:45U0.020 J
Butyl benzyl phthalate 0.020 mg/Kg 0.201 3/7/2015 04:45U0.020 J
Chrysene 0.017 mg/Kg 0.201 3/7/2015 04:45U0.017 J
Di-n-Butyl Phthalate 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
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This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 8 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
SB-4
Matrix:Soil
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847002
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 14:05
Sample Description:Location:
Results for sample J1501847002 are reported on a dry weight basis.
Adjusted
PQL Lab
Di-n-octyl Phthalate 0.030 mg/Kg 0.201 3/7/2015 04:45U0.030 J
Dibenzo[a,h]anthracene 0.021 mg/Kg 0.201 3/7/2015 04:45U0.021 J
Diethyl phthalate 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
Dimethyl phthalate 0.043 mg/Kg 0.201 3/7/2015 04:45I0.024 J
Fluoranthene 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
Fluorene 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
Hexachlorobenzene 0.034 mg/Kg 0.201 3/7/2015 04:45U0.034 J
Hexachlorobutadiene 0.034 mg/Kg 0.201 3/7/2015 04:45U0.034 J
Hexachlorocyclopentadiene 0.020 mg/Kg 0.201 3/7/2015 04:45U0.020 J
Hexachloroethane 0.033 mg/Kg 0.201 3/7/2015 04:45U0.033 J
Indeno(1,2,3-cd)pyrene 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
Isophorone 0.020 mg/Kg 0.201 3/7/2015 04:45U0.020 J
N-Nitrosodi-n-propylamine 0.015 mg/Kg 0.201 3/7/2015 04:45U0.015 J
N-Nitrosodimethylamine 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
N-Nitrosodiphenylamine 0.016 mg/Kg 0.201 3/7/2015 04:45U0.016 J
Naphthalene 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
Nitrobenzene 0.016 mg/Kg 0.201 3/7/2015 04:45U0.016 J
Pentachlorophenol 0.039 mg/Kg 0.201 3/9/2015 19:31U0.039 J
Phenanthrene 0.015 mg/Kg 0.201 3/7/2015 04:45U0.015 J
Phenol 0.020 mg/Kg 0.201 3/7/2015 04:45U0.020 J
Pyrene 0.015 mg/Kg 0.201 3/7/2015 04:45U0.015 J
bis(2-Chloroethoxy)methane 0.019 mg/Kg 0.201 3/7/2015 04:45U0.019 J
bis(2-Chloroethyl)Ether 0.022 mg/Kg 0.201 3/7/2015 04:45U0.022 J
bis(2-Chloroisopropyl) Ether 0.018 mg/Kg 0.201 3/7/2015 04:45U0.018 J
bis(2-Ethylhexyl) phthalate 0.024 mg/Kg 0.201 3/7/2015 04:45U0.024 J
2-Fluorophenol (S)80 %59-1221 3/7/2015 04:45
Phenol-d6 (S)83 %54-1241 3/7/2015 04:45
Nitrobenzene-d5 (S)84 %46-1181 3/7/2015 04:45
2-Fluorobiphenyl (S)59 %54-1341 3/7/2015 04:45
2,4,6-Tribromophenol (S)87 %38-1411 3/7/2015 04:45
p-Terphenyl-d14 (S)88 %60-1431 3/7/2015 04:45
VOLATILES
Analysis Desc: 8260B Analysis, Soil Preparation Method: SW-846 5035
Analytical Method: SW-846 8260B
1,1,1-Trichloroethane 1.4 ug/Kg 3.01 3/3/2015 15:35U1.4 J
1,1,2,2-Tetrachloroethane 2.0 ug/Kg 3.01 3/3/2015 15:35U2.0 J
1,1,2-Trichloroethane 1.4 ug/Kg 3.01 3/3/2015 15:35U1.4 J
1,1-Dichloroethane 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
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Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 9 of 20
ANALYTICAL RESULTS
Workorder:J1501847 Hancock Bank Property
03/02/15 08:54
SB-4
Matrix:Soil
RegLmt
Parameters
Lab ID:
Sample ID:
RegLmt
J1501847002
Results Units
Adjusted
DF AnalyzedMDLQual
Date Collected:
Date Received:
02/28/15 14:05
Sample Description:Location:
Results for sample J1501847002 are reported on a dry weight basis.
Adjusted
PQL Lab
1,1-Dichloroethylene 1.2 ug/Kg 3.01 3/3/2015 15:35U1.2 J
1,2-Dichlorobenzene 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
1,2-Dichloroethane 1.4 ug/Kg 3.01 3/3/2015 15:35U1.4 J
1,2-Dichloropropane 1.2 ug/Kg 3.01 3/3/2015 15:35U1.2 J
1,3-Dichlorobenzene 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
1,4-Dichlorobenzene 1.2 ug/Kg 3.01 3/3/2015 15:35U1.2 J
2-Chloroethyl Vinyl Ether 0.77 ug/Kg 5.01 3/3/2015 15:35U0.77 J
Acrolein (Propenal)4.1 ug/Kg 151 3/3/2015 15:35U4.1 J
Acrylonitrile 5.2 ug/Kg 151 3/3/2015 15:35U5.2 J
Benzene 1.2 ug/Kg 3.01 3/3/2015 15:35U1.2 J
Bromodichloromethane 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
Bromoform 2.0 ug/Kg 5.01 3/3/2015 15:35U2.0 J
Bromomethane 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
Carbon Tetrachloride 1.4 ug/Kg 3.01 3/3/2015 15:35U1.4 J
Chlorobenzene 1.5 ug/Kg 3.01 3/3/2015 15:35U1.5 J
Chloroethane 1.0 ug/Kg 3.01 3/3/2015 15:35U1.0 J
Chloroform 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
Chloromethane 1.0 ug/Kg 3.01 3/3/2015 15:35U1.0 J
Dibromochloromethane 1.3 ug/Kg 3.01 3/3/2015 15:35U1.3 J
Dichlorodifluoromethane 0.85 ug/Kg 3.01 3/3/2015 15:35U0.85 J
Ethylbenzene 1.1 ug/Kg 3.01 3/3/2015 15:35U1.1 J
Methylene Chloride 2.0 ug/Kg 101 3/3/2015 15:35I1.2 J
Tetrachloroethylene (PCE)1.2 ug/Kg 3.01 3/3/2015 15:35U1.2 J
Toluene 1.4 ug/Kg 3.01 3/3/2015 15:35U1.4 J
Trichloroethene 1.0 ug/Kg 3.01 3/3/2015 15:35U1.0 J
Trichlorofluoromethane 0.92 ug/Kg 3.01 3/3/2015 15:35U0.92 J
Vinyl Chloride 1.2 ug/Kg 3.01 3/3/2015 15:35U1.2 J
Xylene (Total)3.8 ug/Kg 9.11 3/3/2015 15:35U3.8 J
cis-1,2-Dichloroethylene 1.4 ug/Kg 3.01 3/3/2015 15:35U1.4 J
cis-1,3-Dichloropropene 1.1 ug/Kg 3.01 3/3/2015 15:35U1.1 J
trans-1,2-Dichloroethylene 0.99 ug/Kg 3.01 3/3/2015 15:35U0.99 J
trans-1,3-Dichloropropylene 0.76 ug/Kg 3.01 3/3/2015 15:35U0.76 J
1,2-Dichloroethane-d4 (S)97 %80-1201 3/3/2015 15:35
Toluene-d8 (S)102 %81-1171 3/3/2015 15:35
Bromofluorobenzene (S)107 %74-1211 3/3/2015 15:35
VOLATILES
Analysis Desc: Percent
Solids,SM2540G,Soil
Analytical Method: SM 2540G
Percent Moisture 15 %1 3/2/2015 10:20 J
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ANALYTICAL RESULTS QUALIFIERS
Workorder:J1501847 Hancock Bank Property
PARAMETER QUALIFIERS
U The compound was analyzed for but not detected.
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
LAB QUALIFIERS
DOH Certification #E82574(AEL-JAX)(FL NELAC Certification)J
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
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QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
QC Batch:
QC Batch Method:
DGMj/1208
SW-846 3010A
Analysis Method:SW-846 6010
Prepared:03/03/2015 03:30
Associated Lab Samples:J1501847001
METHOD BLANK:1690262
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
METALS
Silver 0.00044mg/L 0.00044 U
Arsenic 0.0085mg/L 0.0085 U
Beryllium 0.00013mg/L 0.00013 U
Cadmium 0.00032mg/L 0.00032 U
Chromium 0.00050mg/L 0.00050 U
Copper 0.0025mg/L 0.0025 U
Nickel 0.0011mg/L 0.0011 U
Lead 0.0013mg/L 0.0013 U
Antimony 0.0060mg/L 0.0060 U
Selenium 0.0068mg/L 0.0068 U
Thallium 0.0055mg/L 0.0055 U
Zinc 0.0020mg/L 0.0020 U
QC Batch:
QC Batch Method:
MSVj/1206
SW-846 5035
Analysis Method:SW-846 8260B
Prepared:03/02/2015 09:26
Associated Lab Samples:J1501847002
METHOD BLANK:1690696
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
VOLATILES
Dichlorodifluoromethane 0.84ug/Kg 0.84 U
Chloromethane 1.0ug/Kg 1.0 U
Vinyl Chloride 1.2ug/Kg 1.2 U
Bromomethane 1.3ug/Kg 1.3 U
Chloroethane 1.0ug/Kg 1.0 U
Trichlorofluoromethane 0.91ug/Kg 0.91 U
Acrolein (Propenal)4.1ug/Kg 4.1 U
1,1-Dichloroethylene 1.2ug/Kg 1.2 U
Acrylonitrile 5.2ug/Kg 5.2 U
Methylene Chloride 1.2ug/Kg 1.2 U
trans-1,2-Dichloroethylene 0.98ug/Kg 0.98 U
1,1-Dichloroethane 1.3ug/Kg 1.3 U
cis-1,2-Dichloroethylene 1.4ug/Kg 1.4 U
Chloroform 1.3ug/Kg 1.3 U
1,2-Dichloroethane 1.4ug/Kg 1.4 U
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Report ID: 357001 - 5175626 Page 12 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
METHOD BLANK:1690696
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
1,1,1-Trichloroethane 1.4ug/Kg 1.4 U
Carbon Tetrachloride 1.4ug/Kg 1.4 U
Benzene 1.2ug/Kg 1.2 U
1,2-Dichloropropane 1.2ug/Kg 1.2 U
Trichloroethene 1.0ug/Kg 1.0 U
Bromodichloromethane 1.3ug/Kg 1.3 U
2-Chloroethyl Vinyl Ether 0.76ug/Kg 0.76 U
cis-1,3-Dichloropropene 1.1ug/Kg 1.1 U
trans-1,3-Dichloropropylene 0.75ug/Kg 0.75 U
1,1,2-Trichloroethane 1.3ug/Kg 1.3 U
Toluene 1.4ug/Kg 1.4 U
Dibromochloromethane 1.3ug/Kg 1.3 U
Tetrachloroethylene (PCE)1.2ug/Kg 1.2 U
Chlorobenzene 1.4ug/Kg 1.4 U
Ethylbenzene 1.1ug/Kg 1.1 U
Bromoform 1.9ug/Kg 1.9 U
1,1,2,2-Tetrachloroethane 2.0ug/Kg 2.0 U
1,3-Dichlorobenzene 1.3ug/Kg 1.3 U
1,4-Dichlorobenzene 1.1ug/Kg 1.1 U
1,2-Dichlorobenzene 1.3ug/Kg 1.3 U
Xylene (Total)3.8ug/Kg 3.8 U
1,2-Dichloroethane-d4 (S)97%80-120
Toluene-d8 (S)100%81-117
Bromofluorobenzene (S)104%74-121
QC Batch:
QC Batch Method:
MSVj/1210
SW-846 5030B
Analysis Method:SW-846 8260B
Prepared:03/03/2015 09:49
Associated Lab Samples:J1501847001
METHOD BLANK:1691391
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
VOLATILES
Dichlorodifluoromethane 0.15ug/L 0.15 U
Chloromethane 0.21ug/L 0.21 U
Vinyl Chloride 0.24ug/L 0.24 U
Bromomethane 0.24ug/L 0.24 U
Chloroethane 0.33ug/L 0.33 U
Trichlorofluoromethane 0.32ug/L 0.32 U
Acrolein (Propenal)1.2ug/L 1.2 U
1,1-Dichloroethylene 0.18ug/L 0.18 U
Acrylonitrile 1.1ug/L 1.1 U
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 13 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
METHOD BLANK:1691391
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
Methylene Chloride 1.0ug/L 1.0 U
trans-1,2-Dichloroethylene 0.20ug/L 0.20 U
1,1-Dichloroethane 0.14ug/L 0.14 U
cis-1,2-Dichloroethylene 0.24ug/L 0.24 U
Chloroform 0.18ug/L 0.18 U
1,2-Dichloroethane 0.23ug/L 0.23 U
1,1,1-Trichloroethane 0.22ug/L 0.22 U
Carbon Tetrachloride 0.36ug/L 0.36 U
Benzene 0.21ug/L 0.21 U
1,2-Dichloropropane 0.20ug/L 0.20 U
Trichloroethene 0.29ug/L 0.29 U
Bromodichloromethane 0.25ug/L 0.25 U
2-Chloroethyl Vinyl Ether 0.20ug/L 0.20 U
cis-1,3-Dichloropropene 0.16ug/L 0.16 U
trans-1,3-Dichloropropylene 0.18ug/L 0.18 U
1,1,2-Trichloroethane 0.30ug/L 0.30 U
Toluene 0.23ug/L 0.23 U
Dibromochloromethane 0.33ug/L 0.33 U
Tetrachloroethylene (PCE)0.36ug/L 0.36 U
Chlorobenzene 0.21ug/L 0.21 U
Ethylbenzene 0.24ug/L 0.24 U
Bromoform 0.43ug/L 0.43 U
1,1,2,2-Tetrachloroethane 0.20ug/L 0.20 U
1,3-Dichlorobenzene 0.19ug/L 0.19 U
1,4-Dichlorobenzene 0.22ug/L 0.22 U
1,2-Dichlorobenzene 0.18ug/L 0.18 U
Xylene (Total)0.53ug/L 0.53 U
1,2-Dichloroethane-d4 (S)112%80-120
Toluene-d8 (S)102%88-110
Bromofluorobenzene (S)105%86-115
QC Batch:
QC Batch Method:
DGMj/1211
SW-846 3050B
Analysis Method:SW-846 6010
Prepared:03/04/2015 10:19
Associated Lab Samples:J1501847002
METHOD BLANK:1691932
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
METALS
Silver 0.0012mg/Kg 0.0012 U
Arsenic 0.0091mg/Kg 0.0091 U
Beryllium 0.000086mg/Kg 0.000086 U
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 14 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
METHOD BLANK:1691932
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
Cadmium 0.0013mg/Kg 0.0013 U
Chromium 0.0024mg/Kg 0.0024 U
Copper 0.0022mg/Kg 0.0022 U
Nickel 0.0019mg/Kg 0.0019 U
Lead 0.0020mg/Kg 0.0020 U
Selenium 0.0075mg/Kg 0.0075 U
Thallium 0.0052mg/Kg 0.0052 U
Zinc 0.0075mg/Kg 0.0075 U
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
METALS
Antimony 0.0049mg/Kg 0.0049 U
QC Batch:
QC Batch Method:
EXTj/1252
SW-846 3550B
Analysis Method:SW-846 8270C
Prepared:03/05/2015 09:00
Associated Lab Samples:J1501847002
METHOD BLANK:1693431
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
SEMIVOLATILES
Phenol 0.017mg/Kg 0.017 U
2-Chlorophenol 0.016mg/Kg 0.016 U
2-Nitrophenol 0.015mg/Kg 0.015 U
2,4-Dimethylphenol 0.016mg/Kg 0.016 U
2,4-Dichlorophenol 0.022mg/Kg 0.022 U
4-Chloro-3-methylphenol 0.013mg/Kg 0.013 U
2,4,6-Trichlorophenol 0.019mg/Kg 0.019 U
2,4-Dinitrophenol 0.055mg/Kg 0.055 U
4-Nitrophenol 0.041mg/Kg 0.041 U
2-Methyl-4,6-dinitrophenol 0.037mg/Kg 0.037 U
Pentachlorophenol 0.033mg/Kg 0.033 U
N-Nitrosodimethylamine 0.016mg/Kg 0.016 U
bis(2-Chloroethyl)Ether 0.018mg/Kg 0.018 U
1,3-Dichlorobenzene 0.021mg/Kg 0.021 U
1,4-Dichlorobenzene 0.025mg/Kg 0.025 U
1,2-Dichlorobenzene 0.023mg/Kg 0.023 U
bis(2-Chloroisopropyl) Ether 0.015mg/Kg 0.015 U
N-Nitrosodi-n-propylamine 0.013mg/Kg 0.013 U
Hexachloroethane 0.028mg/Kg 0.028 U
Nitrobenzene 0.013mg/Kg 0.013 U
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 15 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
METHOD BLANK:1693431
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
Isophorone 0.017mg/Kg 0.017 U
bis(2-Chloroethoxy)methane 0.016mg/Kg 0.016 U
1,2,4-Trichlorobenzene 0.022mg/Kg 0.022 U
Naphthalene 0.015mg/Kg 0.015 U
Hexachlorobutadiene 0.028mg/Kg 0.028 U
Hexachlorocyclopentadiene 0.017mg/Kg 0.017 U
2-Chloronaphthalene 0.018mg/Kg 0.018 U
Dimethyl phthalate 0.021mg/Kg 0.021 U
2,6-Dinitrotoluene (2,6-DNT)0.027mg/Kg 0.027 U
Acenaphthylene 0.013mg/Kg 0.013 U
Acenaphthene 0.016mg/Kg 0.016 U
2,4-Dinitrotoluene (2,4-DNT)0.018mg/Kg 0.018 U
Diethyl phthalate 0.015mg/Kg 0.015 U
Fluorene 0.016mg/Kg 0.016 U
4-Chlorophenyl Phenyl Ether 0.025mg/Kg 0.025 U
1,2-Diphenylhydrazine 0.013mg/Kg 0.013 U
4-Bromophenyl Phenyl Ether 0.023mg/Kg 0.023 U
Hexachlorobenzene 0.028mg/Kg 0.028 U
Phenanthrene 0.012mg/Kg 0.012 U
Anthracene 0.014mg/Kg 0.014 U
Di-n-Butyl Phthalate 0.015mg/Kg 0.015 U
Fluoranthene 0.016mg/Kg 0.016 U
Benzidine 0.012mg/Kg 0.012 U
Pyrene 0.013mg/Kg 0.013 U
Butyl benzyl phthalate 0.017mg/Kg 0.017 U
Benzo[a]anthracene 0.014mg/Kg 0.014 U
3,3`-Dichlorobenzidine 0.025mg/Kg 0.025 U
Chrysene 0.014mg/Kg 0.014 U
bis(2-Ethylhexyl) phthalate 0.020mg/Kg 0.020 U
Di-n-octyl Phthalate 0.025mg/Kg 0.025 U
Benzo[b]fluoranthene 0.013mg/Kg 0.013 U
Benzo[k]fluoranthene 0.017mg/Kg 0.017 U
Benzo[a]pyrene 0.015mg/Kg 0.015 U
Indeno(1,2,3-cd)pyrene 0.016mg/Kg 0.016 U
Dibenzo[a,h]anthracene 0.017mg/Kg 0.017 U
Benzo[g,h,i]perylene 0.018mg/Kg 0.018 U
N-Nitrosodiphenylamine 0.014mg/Kg 0.014 U
2-Fluorophenol (S)89%59-122
Phenol-d6 (S)82%54-124
Nitrobenzene-d5 (S)83%46-118
2-Fluorobiphenyl (S)81%54-134
2,4,6-Tribromophenol (S)72%38-141
p-Terphenyl-d14 (S)85%60-143
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 16 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
QC Batch:
QC Batch Method:
EXTj/1259
SW-846 3510C
Analysis Method:SW-846 8270C
Prepared:03/05/2015 17:30
Associated Lab Samples:J1501847001
METHOD BLANK:1694631
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
SEMIVOLATILES
Phenol 0.54ug/L 0.54 U
2-Chlorophenol 1.2ug/L 1.2 U
2-Nitrophenol 0.63ug/L 0.63 U
2,4-Dimethylphenol 2.6ug/L 2.6 U
2,4-Dichlorophenol 0.90ug/L 0.90 U
4-Chloro-3-methylphenol 0.62ug/L 0.62 U
2,4,6-Trichlorophenol 0.93ug/L 0.93 U
2,4-Dinitrophenol 0.62ug/L 0.62 U
4-Nitrophenol 0.62ug/L 0.62 U
2-Methyl-4,6-dinitrophenol 0.77ug/L 0.77 U
Pentachlorophenol 0.95ug/L 0.95 U
N-Nitrosodimethylamine 0.62ug/L 0.62 U
bis(2-Chloroethyl)Ether 1.5ug/L 1.5 U
1,3-Dichlorobenzene 1.0ug/L 1.0 U
1,4-Dichlorobenzene 1.2ug/L 1.2 U
1,2-Dichlorobenzene 1.4ug/L 1.4 U
bis(2-Chloroisopropyl) Ether 1.4ug/L 1.4 U
N-Nitrosodi-n-propylamine 2.2ug/L 2.2 U
Hexachloroethane 1.2ug/L 1.2 U
Nitrobenzene 1.1ug/L 1.1 U
Isophorone 1.1ug/L 1.1 U
bis(2-Chloroethoxy)methane 1.2ug/L 1.2 U
1,2,4-Trichlorobenzene 0.69ug/L 0.69 U
Naphthalene 1.2ug/L 1.2 U
Hexachlorobutadiene 0.87ug/L 0.87 U
Hexachlorocyclopentadiene 0.99ug/L 0.99 U
2-Chloronaphthalene 0.97ug/L 0.97 U
Dimethyl phthalate 1.4ug/L 1.4 U
2,6-Dinitrotoluene (2,6-DNT)1.1ug/L 1.1 U
Acenaphthylene 0.84ug/L 0.84 U
Acenaphthene 0.96ug/L 0.96 U
2,4-Dinitrotoluene (2,4-DNT)0.60ug/L 0.60 U
Diethyl phthalate 0.98ug/L 0.98 U
Fluorene 0.85ug/L 0.85 U
4-Chlorophenyl Phenyl Ether 0.69ug/L 0.69 U
1,2-Diphenylhydrazine 0.96ug/L 0.96 U
4-Bromophenyl Phenyl Ether 1.1ug/L 1.1 U
Hexachlorobenzene 0.99ug/L 0.99 U
Phenanthrene 0.55ug/L 0.55 U
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
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CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 17 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
METHOD BLANK:1694631
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
Anthracene 0.50ug/L 0.50 U
Di-n-Butyl Phthalate 0.88ug/L 0.88 U
Fluoranthene 0.64ug/L 0.64 U
Benzidine 0.74ug/L 0.74 U
Pyrene 0.59ug/L 0.59 U
Butyl benzyl phthalate 1.1ug/L 1.1 U
Benzo[a]anthracene 0.54ug/L 0.54 U
3,3`-Dichlorobenzidine 1.3ug/L 1.3 U
Chrysene 0.67ug/L 0.67 U
bis(2-Ethylhexyl) phthalate 1.4ug/L 1.4 U
Di-n-octyl Phthalate 1.2ug/L 1.2 U
Benzo[b]fluoranthene 0.77ug/L 0.77 U
Benzo[k]fluoranthene 0.70ug/L 0.70 U
Benzo[a]pyrene 0.58ug/L 0.58 U
Indeno(1,2,3-cd)pyrene 0.68ug/L 0.68 U
Dibenzo[a,h]anthracene 0.73ug/L 0.73 U
Benzo[g,h,i]perylene 0.76ug/L 0.76 U
N-Nitrosodiphenylamine 0.59ug/L 0.59 U
2-Fluorophenol (S)62%10-90
Phenol-d6 (S)43%10-67
Nitrobenzene-d5 (S)98%32-147
2-Fluorobiphenyl (S)105%34-140
2,4,6-Tribromophenol (S)113%19-190
p-Terphenyl-d14 (S)112%54-138
QC Batch:
QC Batch Method:
DGMj/1216
SW-846 7471A
Analysis Method:SW-846 7471A
Prepared:03/06/2015 08:48
Associated Lab Samples:J1501847002
METHOD BLANK:1694659
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
METALS
Mercury 0.00042mg/Kg 0.00042 U
QC Batch:
QC Batch Method:
DGMj/1237
SW-846 7470A
Analysis Method:SW-846 7470A
Prepared:03/09/2015 09:35
Associated Lab Samples:J1501847001
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
without the written consent of Advanced Environmental Laboratories, Inc.
3004.1.0.0
Advanced Environmental Laboratories, Inc
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
Report ID: 357001 - 5175626 Page 18 of 20
QUALITY CONTROL DATA
Workorder:J1501847 Hancock Bank Property
METHOD BLANK:1696093
Parameter Units Result
Blank
Limit
Reporting
Qualifiers
METALS
Mercury 0.000010mg/L 0.000010 U
QUALITY CONTROL DATA QUALIFIERS
Workorder:J1501847 Hancock Bank Property
QUALITY CONTROL PARAMETER QUALIFIERS
U The compound was analyzed for but not detected.
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
Lab QC FailureJ3
Estimated ResultJ4
[]
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
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CERTIFICATE OF ANALYSIS
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Report ID: 357001 - 5175626 Page 19 of 20
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder:J1501847 Hancock Bank Property
Lab ID Sample ID Prep Method Analysis MethodPrep Batch Batch
Analysis
J1501847002 SB-4 WCAj/1333SM 2540G
J1501847001 DGMj/1208GW-1 ICPj/1129SW-846 3010A SW-846 6010
J1501847002 MSVj/1206SB-4 MSVj/1207SW-846 5035 SW-846 8260B
J1501847001 MSVj/1210GW-1 MSVj/1211SW-846 5030B SW-846 8260B
J1501847002 DGMj/1211SB-4 ICPj/1133SW-846 3050B SW-846 6010
J1501847002 EXTj/1252SB-4 MSSj/1122SW-846 3550B SW-846 8270C
J1501847001 EXTj/1259GW-1 MSSj/1120SW-846 3510C SW-846 8270C
J1501847002 DGMj/1216SB-4 CVAj/1038SW-846 7471A SW-846 7471A
J1501847001 DGMj/1237GW-1 CVAj/1041SW-846 7470A SW-846 7470A
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
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3004.1.0.0
Page 20 of 20
Tuesday, March 10, 2015 11:00:45 AM