Environmental Site Assessment Report Phase 2 (March 2015)PHASE II ENVIRONMENTAL
SITE ASSESSMENT REPORT
Of
Parcel RE #170891-0000
West 6th Street & Jasmine Street
Atlantic Beach, Duval County, Florida
(PES Project #150204)
Prepared for:
Sessa Properties, LLC
9378 Arlington Expressway, Suite 315
Jacksonville, Florida 32225
Prepared by:
Pfahler Environmental Services, Inc.
1212 Forest Oaks Drive
Neptune Beach, Florida 32266
March 2015
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY....................................................................................1
2.0 INTRODUCTION................................................................................................ 3
2.1 Purpose...................................................................................................... 3
2.2 Scope of Services...................................................................................... 3
2.3 Limiting Conditions and Methodologies Used.............................................4
3.0 PROPERTYBACKGROUND............................................................................5
3.1 Property Location and Description............................................................. 5
3.2 Physical Setting..........................................................................................5
3.3 Current Use and Site Improvements.......................................................... 5
3.4 Adjoining Property Use............................................................................... 5
4.0 PHASE II ACTIVITIES....................................................................................... 6
4.1 Scope of Assessment................................................................................. 6
4.1.1 Supplemental Record Review......................................................... 6
4.1.2 Chemical Testing Plan.....................................................................6
4.1.3 Deviations from the Work Plan ........................................................ 6
4.2 Field Sampling and Methods......................................................................6
4.2.1 Soil Sample Collection and Soil -Vapor Screening ........................... 6
4.2.2 Groundwater Sample Collection...................................................... 7
4.3 Sample Analyses........................................................................................ 7
4.3.1 Soil................................................................................................... 7
4.3.2 Groundwater....................................................................................7
5.0 EVALUATION AND PRESENTATION OF RESULTS.......................................8
5.1 Subsurface Conditions............................................................................... 8
5.1.1 Geologic Setting.............................................................................. 8
5.1.2 Hydrogeologic Conditions................................................................ 8
5.2 Field and Analytical Data Results............................................................... 8
5.2.1 Soil Vapor Screening Results..........................................................8
5.2.3 Groundwater....................................................................................9
6.0 CONCLUSIONS AND RECOMMENDATIONS................................................10
7.0 CLOSURE........................................................................................................11
8.0 REFERENCES.................................................................................................12
Page i
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
Figures
Figure 1 - Property Location Map
Figure 2 - Sampling Location Map
Tables
Table 1 - Soil Vapor Screening Data Summary
Table 2 - Soil Analytical Data Summary
Table 3 - Groundwater Analytical Data Summary
Appendices
APPENDIX A - Soil Boring Logs
APPENDIX B - Analytical Laboratory Report
Page ii
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
1.0 EXECUTIVE SUMMARY
Sessa Properties, LLC (Client) engaged Pfahler Environmental Services, Inc. (PES) to
conduct a Phase II Environmental Site Assessment (ESA) of Parcel RE #170891-0000
located at the southwestern quadrant of West 6th Street and Jasmine Street in Atlantic
Beach, Duval County, Florida, subsequently referred to in this report as "the property'.
The Phase II ESA was competed in general accordance with the American Society of
Testing and Materials (ASTM) Standard Practice for Environmental Site Assessments:
Phase II ESA Process (ASTM Designation: E1903-11) and applicable criteria provided
in Florida Department of Environmental Protection (FDEP) Chapter 62-780, Florida
Administrative Code (FAC).
The purpose of the Phase II ESA is to further evaluate the recognized environmental
conditions (RECs) and Business Environmental Risks (BERs) identified in the previous
Phase I ESA report. The goal is to collect sufficient information to determine the
presence or absence of impacted soil and/or groundwater at the property. The Phase
I ESA report (dated February 8, 2015) prepared by PES identified the following:
➢ REC 1 - The 1943 and 1960 historical aerial photographs show a marsh at the
southern half of the property. The 1970 aerial photograph shows that the
ground surface of the property had been completely reworked and appears to
have included filling in the previously noted marsh. The southern half of the
property may have been impacted by a former old dump reportedly operated by
the City of Atlantic Beach in the 1960s and 1970s at the south and west
adjoining properties. Reportedly solid waste was originally brought onto the
properties to fill in wetlands and low areas followed with some trenching and
above grade trash disposal. The likely presence of unknown buried solid waste
at the property is considered a moderate to high environmental risk.
➢ BER 1 — PES observed used tires and solid waste dumped on the ground
surface, and visible evidence of buried solid waste at the southern half of the
property. Removal and proper disposal of the waste would be necessary
before the property is suitable for development.
Scope of Work. The Phase II investigation tasks performed to further evaluate the
subsurface condition of the property included installation of five (5) soil borings and
one groundwater probe well using a Geoprobe 7822DT, collection of soil samples for
field soil -vapor screening and chemical analysis, collection of groundwater sample for
chemical analysis, and evaluation of investigative data and preparation of final report.
Sampling Results. No visible evidence of free product or visibly stained soil was
observed during drilling of the boreholes. Soil samples were collected from the
vadose and water table zones at boring locations SB -1 through SB -5 and field -
screened for volatile organic vapors with an Organic Vapor Analyzer (OVA) to identify
any potential soil contamination and assist with determining the ideal location of the
groundwater sampling point. No positive OVA readings were detected in any of the
soil samples collected from borings, except for concentration of 0.3 ppm at a depth of
Page 1 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
10.0 feet BLS of boring SB -4. Because of the lack of positive OVA readings in the
soil -vapor screening, the soil sample for chemical analysis was collected from a depth
interval of 2.0-3.0 feet BLS at boring location SB4. Analytical results for soil sample
SB -4 indicated no contaminants of concern (COC) concentrations except for the
following:
•
134— Methylene Chloride 2 milligrams per kilogram (mg/kg), Dimethyl
phthalate at 0.043 mg/kg, Beryllium at 0.058 mg/kg, Cadmium at 0.14
mg/kg, Chromium at 2.9 mg/kg, Copper at 35 mg/kg, Lead at 5.5 mg/kg,
Nickel at 2.1 mg/kg, Zinc at 35 mg/kg, and Mercury at 0.023 mg/kg.
PES selected boring location SB -3 as the groundwater sampling point. A Geoprobe
direct -push technology rig was used to collect groundwater sample GW -1 from a depth
of 12 feet below land surface (BLS). No visible evidence of free product or suspicious
sheen was observed in the groundwater probe well during sample collection.
Analytical results for groundwater sample GW -1 indicated no COC concentrations
except for the following:
• GW -1 — 1,4-Dichlorobenene at 1.1 micrograms per liter (Ng/L), Chlorobenzene
at 6 pg/L, Beryllium at 0.0008 milligrams per liter (mg/L), Chromium at
0.017 mg/L, Lead at 0.011 mg/L, Nickel at 0.0029 mg/L, Silver at
0.0015 mg/L, and Mercury at 0.000063 mg/L.
Conclusions. Based on the findings of this investigation, PES's conclusions are as
follows:
- Results of the soil -vapor screening indicated no evidence of soil contamination
in the vadose and water table zones at the boring locations of this investigation.
In addition, although the analytical results indicated detectable COC
concentrations in soil boring SB -4, none of the concentrations are above the
SCTLs provided in FDEP Chapter 62-777, FAC.
Although the analytical results of the chemical analysis indicated detectable
COC concentrations in groundwater sample GW -1, none of the concentrations
exceed the GCTLs provided in FDEP Chapter 62-777, FAC.
In our opinion, this Phase II ESA has adequately addressed the REC and BER that
were the subject of this investigation, and that further site assessment of the
subsurface soil and groundwater quality is not warranted for the property at this time.
With regards to the buried solid waste identified at the property, further action that
most likely would involve the removal and off-site disposal of the waste material, and
replacement with clean soil should be considered to assure there is a ground surface
suitable for building construction.
Page 2 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
2.0 INTRODUCTION
Sessa Properties, LLC (Client) engaged Pfahler Environmental Services, Inc. (PES)
to conduct a Phase II Environmental Site Assessment (ESA) of Parcel RE #170891-
0000 located at the southwestern quadrant of West 6th Street and Jasmine Street in
Atlantic Beach, Duval County, Florida, subsequently referred to in this report as "the
property'. The Phase II assessment was completed in general accordance with the
American Society of Testing and Materials (ASTM) Standard Practice for
Environmental Site Assessments: Phase II ESA Process (ASTM Designation: E1903-
11) and applicable criteria provided in Florida Department of Environmental Protection
(FDEP) Chapter 62-780, Florida Administrative Code (FAC). This report summarizes
the field activities and findings of our investigation.
2.1 Purpose
The purpose of the Phase II ESA is to further evaluate the recognized environmental
conditions (RECs) and Business Environmental Risks (BERs) identified in the previous
Phase I ESA report. The goal is to collect sufficient information to determine the
presence or absence of impacted soil and/or groundwater at the property. The Phase
I ESA report (dated February 8, 2015) prepared by PES identified the following:
➢ REC 1 - The 1943 and 1960 historical aerial photographs show a marsh at the
southern half of the property. The 1970 aerial photograph shows that the
ground surface of the property had been completely reworked and appears to
have included filling in the previously noted marsh. The southern half of the
property may have been impacted by a former old dump reportedly operated by
the City of Atlantic Beach in the 1960s and 1970s at the south and west
adjoining properties. Reportedly solid waste was originally brought onto the
properties to fill in wetlands and low areas followed with some trenching and
above grade trash disposal. The likely presence of unknown buried solid waste
at the property is considered a moderate to high environmental risk.
➢ BER 1 — PES observed used tires and solid waste dumped on the ground
surface, and visible evidence of buried solid waste at the southern half of the
property. Removal and proper disposal of the waste would be necessary
before the property is suitable for development.
2.2 Scope of Services
Based on the findings of PES's Phase I ESA, the Phase II scope of services included
the following tasks:
• Installation of soil borings at select areas of the property
• Field screening of collected soil samples for volatile organic vapors
• Collection and chemical analyses of soil and groundwater samples
• Evaluation of field observations and sampling results
• Evaluation of the investigative data and preparation of final report
Page 3 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
2.3 Limiting Conditions and Methodologies Used
No assessment can eliminate all uncertainty. Furthermore, any sample, either surface
or subsurface taken for chemical analysis may or may not represent a larger
population. Professional judgment and interpretation are inherent in the process and
uncertainty is possible. The number of sampling points may be able to reduce the
uncertainty but at the same time increase the cost of the assessment.
Even when a Phase II ESA is executed with an appropriate site-specific standard of
care, certain conditions present especially difficult detection problems. Such
conditions may include, but are not limited to, complex geological settings, the fate and
transport characteristics of certain hazardous substances and petroleum products, the
distribution of existing contamination, physical limitations imposed by the location of
utilities and other man-made objects, and the limitations of assessment technologies.
A Phase II ESA does not generally require an exhaustive assessment of
environmental conditions on a property. There is a point at which the cost and time
required to obtain the information outweighs the usefulness of that information and, in
fact, may be a material detriment to the orderly completion of real estate transactions.
If hazardous substance or petroleum releases are confirmed on a parcel of property,
the extent of further assessment to delineate the release is related to the degree of
uncertainty that is acceptable to the user with respect to the transaction.
Field measurements and analytical data only represent the site conditions at the time
of sample collection. Therefore, the usability of data collected as part of this Phase II
ESA may have a finite usefulness depending on the application and use being made
of the data. An environmental professional should evaluate whether the generated
data are appropriate for any subsequent use beyond the original purpose for which the
data was collected.
Page 4 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
3.0 PROPERTY BACKGROUND
3.1 Property Location and Description
The property is located at southwestern quadrant of the intersection of West 6th Street
and Jasmine Street, which is situated in Northwest '/4 of the Northwest '/4 of Section
38, Township 2 South, Range 29 East of Atlantic Beach, Duval County, Florida. The
property location is shown on Figure 1.
According to the Duval County Property Appraiser (DCPA) records, property details
are as follows:
• Owner: Hancock Bank
• RE #: 170891-0000
• Property Use: Vacant Residential (0.515 acres) and Jurisdictional Wetlands
(0.11 acres)
• Zoning: ARS -2 (Residential Single Atlantic Beach)
• Land Units: 0.625 acres
3.2 Physical Setting
Topography at the property ranges between 5 feet and 10 feet National Geodetic
Vertical Datum (NGVD). On inspection, the property was observed to be relatively flat
with some undulations (particularly in the southern half) and several areas of subtle
mounding.
Shallow groundwater can be found at a depth of 4 feet below land surface (BLS) or
less and apparently flows in westerly direction towards nearby Intracoastal Waterway.
However, the direction of flow may vary at times due to influence from tidal
fluctuations.
3.3 Current Use and Site Improvements
The property is currently vacant with no identifiable improvements.
3.4 Adjoining Property Use
Adjoining property uses include Residential - single-family beyond 6th Street to the
north; Vacant Residential — auto salvage storage yard to the south; Residential —
single family beyond (unpaved) Jasmine Street to the east; and, Light Industrial — auto
salvage open storage yard to the west.
Page 5 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
4.0 PHASE II ACTIVITIES
4.1 Scope of Assessment
4.1.1 Supplemental Record Review
Aside from our review of the Phase I ESA report prepared by PES, no supplemental
environmental records were reviewed as part of this Phase II ESA.
4.1.2 Chemical Testing Plan
The analytical testing plan was designed to detect the contaminants suspected to be
present in the samples collected. This testing plan included tests which provide quality
assurance (QA) and techniques that provide quality control (QC) over the chemical
analysis. A completed chain of custody record accompanied each sample shipment to
the analytical laboratory. Chain of custody records provide written documentation
regarding sample collection and handling, identify the persons involved in the chain of
sample possession, and a written record of requested analytical parameters.
4.1.3 Deviations from the Work Plan
There were no deviations to the proposed work plan of this Phase II investigation.
4.2 Field Sampling and Methods
PES and Probe Domain (subcontract driller) personnel initiated and completed the
field sampling activities on February 28, 2015. Following the collection of soil and
groundwater samples, all boreholes were backfilled with the soil drill cuttings.
4.2.1 Soil Sample Collection and Soil -Vapor Screening
Probe Domain utilized a Geoprobe 7822DT direct -push technology (DPT) rig to install
five (5) soil borings (- through SB -5) to a depth of 10.0 feet below land surface (BLS)
at the locations shown on Figure 2. The DPT rig hydraulically advanced a 2.25 -inch
outside diameter five-foot long carbon steel core barrel equipped with an acrylic inner
sleeve continuously to the required depth at each boring location. The acrylic sleeve
of each core barrel was removed and cut open to expose a 1.125 -inch soil core. PES
personnel hand -grabbed soil samples from the cores representing depths 2.0 feet, 4.0
feet, 6.0 feet, and at 10.0 feet BLS, and placed the samples into glass mason jars
(filled to one-half capacity) and sealed the jars with aluminum foil.
Soils collected for chemical analysis were hand -grabbed and placed directly into the
laboratory -supplied containers, except for volatile analysis an Encor (secondary
device) sampler was used to fill the containers. The sample containers were placed
with wet ice in a hard shell cooler and transported along with chain -of -custody to
Advanced Environmental Laboratory (AEL) in Jacksonville.
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Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
4.2.2 Groundwater Sample Collection
Based on the soil -vapor screening results and field observations, PES selected boring
SB -3 as the location to collect the groundwater sample (GW -1). Sample location is
shown on Figure 2. Probe Domain used the Geoprobe to hydraulically advance a 4 -
foot long stainless steel screen with 0.006 -inch slots that was flush -threaded to carbon
steel push rods to a depth of 12.0 feet BLS. Once the probe well was pushed to the
desired depth, the drill rod was retracted four feet to expose the screen section to the
aquifer. PES personnel then developed the probe well using a peristaltic pump to
remove unwanted sediment and to establish a hydraulic connection with the aquifer.
Following the well development the aquifer was allowed time to stabilize to static
conditions before sample collection. PES personnel used the peristaltic pump to
collect groundwater sample GW -1 by directly filling the laboratory -supplied containers
using the after -pump method. Sample bottles designated for volatile organics analysis
were filled first followed with filling the containers for semi -volatile organics and metals
analyses.
4.3 Sample Analyses
4.3.1 Soil
Soil -Vapor Screening. The soil samples were allowed to equilibrate to the ambient air
temperature before being field -screened using a MiniRAE 3000 Organic Vapor
Analyzer (OVA), equipped with a photo ionization detector (PID). A total of 20 soil
samples were field -screened with the OVA to determine the presence or absence of
volatile organic vapors in the vadose (unsaturated) and water table (saturated) zones.
The screening process involved piercing the aluminum foil seal of a mason jar with the
OVA probe and obtaining a vapor aliquot from the jar's headspace. The OVA provided
a direct reading of the vapor concentration in parts per million (ppm).
Chemical
Analysis. Since no positive OVA
readings were detected in
the soil
samples,
PES selected soil boring SB -4 for
chemical analysis based
on field
observations. Requested analysis included
Priority Pollutant Volatile
Organics
(PPVOs)
using EPA Method 8260B, Priority Pollutant Semi -Volatile
Organics
(PPSVOs)
using EPA Method 8270 -SIM, and
Priority Pollutant Metals using EPA
Methods 6010
and 7470.
4.3.2 Groundwater
The sample containers were placed with wet ice in a hard shell cooler and transported
along with chain -of -custody to AEL. Requested analyses of groundwater sample GW -
1 included PPVOs using EPA Method 8260B, PPSVOs using EPA Method 8270 -SIM,
and Priority Pollutant Metals using EPA Methods 6010 and 7470.
Page 7 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
5.0 EVALUATION AND PRESENTATION OF RESULTS
5.1 Subsurface Conditions
5.1.1 Geologic Setting
As described through observation of the soil cores, the site-specific lithology consists
of 4-5 feet of loose orangish brown -brown -grayish brown -light brown sand (fill) with a
2 -foot layer of brown -dark brown silty sand at boring SB -3. Followed by 2.5-4 feet of
buried solid waste at the borings, except for boring SB -1 where only a thin (1-2 inches)
lens of debris was encountered at a depth of 4.5-5 feet BLS. A one foot layer of black
sandy silt (muck) was encountered at a depth of 7.0 feet BLS at boring SB -4. These
layers are underlain by either light brown -gray sand or light gray -gray sandy clayey silt
to the end of the borings except for boring SB -1 where brown -gray and dark brown
silty sand was encountered from 7.5 feet BLS to the end of boring.
Solid waste observed soil cores collected from the soil borings (SB -1 through S-5)
consisted of domestic trash, such as paper, plastic, Styrofoam, and glass and wood
which was observed in soil samples collected borings SB -3 and SB -4. Only a thin lens
(1-2 inches) of trash was observed at a depth of 4.5-5 feet BLS of boring SB -1. Based
on the soil cores and our field observations, the buried solid waste appears to be
located in the southern two-thirds of the property. Lithologic descriptions are included
in the soil boring logs provided in Appendix A.
5.1.2 Hydrogeologic Conditions
No surface water features were identified at the property or adjoining properties,
except for drainage ditches along the southern and western boundaries. Surface
water features found in the surrounding area include a tidal marsh approximately 100
feet southeast, two retention ponds 575 feet south, Intracoastal Waterway less than
1,000 feet west and Hopkins Creek approximately 2800 feet east of the property.
Groundwater was encountered in the soil borings at depths between 3.0 feet and 3.5
feet BLS.
5.2 Field and Analytical Data Results
5.2.1 Soil Vapor Screening Results
No visible evidence of free product or visibly stained soil was observed during drilling
of the boreholes. Soil samples were collected from the vadose and water table zones
at boring locations SB -1 through SB -5. The samples were field -screened for volatile
organic vapors with the OVA to identify any potential soil contamination and assist with
determining the ideal location of the groundwater sampling point. No positive OVA
readings were detected in any of the soil samples collected from borings, except for
concentration of 0.3 ppm at a depth of 10.0 feet BLS of boring SB -4. Soil sampling
depths and OVA readings are presented in Table 1 and on the boring logs provided in
Appendix A.
Page 8 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
5.2.2 Soil Analytical Results
Because of the lack of positive OVA readings in the soil -vapor screening, the soil
sample for chemical analysis was collected from a depth interval of 2.0-3.0 feet BLS at
boring location SB4. The sample was submitted to AEL for chemical analysis.
Analytical results for soil sample SB -4 indicated no contaminants of concern (COC)
concentrations except for the following:
134 — Methylene Chloride 2 milligrams per kilogram (mg/kg), Dimethyl
phthalate at 0.043 mg/kg, Beryllium at 0.058 mg/kg, Cadmium at 0.14
mg/kg, Chromium at 2.9 mg/kg, Copper at 35 mg/kg, Lead at 5.5 mg/kg,
Nickel at 2.1 mg/kg, Zinc at 35 mg/kg, and Mercury at 0.023 mg/kg.
Soil analytical results along with the applicable FDEP Soil Cleanup Target Levels
(SCTLs) are summarized in Tables 2, 3 and 4. The analytical laboratory report is
provided as Appendix B.
5.2.3 Groundwater
No visible evidence of free product or suspicious sheen was observed in the
groundwater probe well (GW -1) during sample collection. Analytical results for
groundwater sample GW -1 indicated no COC concentrations except for the following:
GW -1 — 1,4-Dichlorobenene at 1.1 micrograms per liter (Ng/L), Chlorobenzene
at 6 pg/L, Beryllium at 0.0008 milligrams per liter (mg/L), Chromium at
0.017 mg/L, Lead at 0.011 mg/L, Nickel at 0.0029 mg/L, Silver at
0.0015 mg/L, and Mercury at 0.000063 mg/L.
The groundwater analytical results along with the applicable FDEP Groundwater
Cleanup Target Levels (GCTLs) are summarized in Tables 5, 6 and 7. The analytical
laboratory report is provided as Appendix B.
Page 9 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
6.0 CONCLUSIONS AND RECOMMENDATIONS
This Phase II ESA was completed in general accordance with environmental
methodologies referred to in ASTM Practice E1903-11 and applicable site assessment
criteria provided in FDEP Chapter 62-780, FAC, and contains all of the limitations
inherent in these methodologies. No other warranties, expressed or implied, are made
as to the professional services provided under the terms of our contract and included
in this report. Based on the findings of this investigation, PES's conclusions are as
follows:
➢ Soil. Results of the soil -vapor screening indicated no evidence of soil
contamination in the vadose and water table zones at the boring locations of
this investigation. In addition, although the analytical results indicated
detectable COC concentrations in soil boring SB -4, none of the concentrations
are above the SCTLs provided in FDEP Chapter 62-777, FAC.
➢ Groundwater. Although the analytical results of the chemical analysis indicated
detectable COC concentrations in groundwater sample GW -1, none of the
concentrations are above the GCTLs provided in FDEP Chapter 62-777, FAC.
In our opinion, this Phase II ESA has adequately addressed the REC and BER that
were the subject of this investigation, and that further site assessment of the
subsurface soil and groundwater quality is not warranted for the property at this time.
With regards to the buried solid waste identified at the property, further action that
most likely would involve the removal and off-site disposal of the waste material, and
replacement with clean soil should be considered to assure there is a ground surface
suitable for building construction.
Page 10 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
7.0 CLOSURE
This report has been prepared for the sole benefit of Sessa Properties, LLC, and their
successors and assigns. The report may not be relied upon by any other person or
entity without the express written consent of PES.
Respectfully submitted,
PFAHLER ENVIRONMENTAL SERVICES, INC.
Randall o,W;,.�,
�.
F. Pfahlerc�"""..
Randall F. Pfahler, PG #1362
Principal Consultant
Date: March 10, 2015
Page 11 of 12
Parcel RE #170891-0000
Phase II ESA Report
PES Project #150204
8.0 REFERENCES
The following references may have been used in the preparation of this report.
• ASTM Standard D 5730 Guide to Site Characteristics for Environmental
Purposes With Emphasis on Soil, Rock, The Vadose Zone and Ground Water
• ASTM Standard E 1903-11 Standard Practice for Environmental Site
Assessments: Phase II Environmental Site Assessment Process
• FDEP Contaminant Cleanup Target Levels — Chapter 62-777, FAC
• FDEP Contaminated Site Cleanup Criteria — Chapter 62-780, FAC
Page 12 of 12
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PFAHLER ENVIRONMENTAL Figure 1
SERVICES, INC. PARCEL RE #170891-0000 PROPERTY LOCATION MAP
West 6th Street and Jasmine Street PROJECT NO.: DRAWN BY:
1212 Forest Oaks Drive 150205
Neptune Beach, Florida 32266 Atlantic Beach, Florida DATE: SCALD:
P � 3/3/15 1 1' = 2000 FEET
WEST 6TH STREET
T.--.-PROPERTYLINE
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19 Approximate Location of Groundwater Sample/Soil Boring
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Florida Department of Environmental Protection — Bureau of Petroleum Storage Systems — Preapproval Program — Site Assessment
Reporting
TABLE 1: Soil -Vapor Screening Data Summary
Site Name: Parcel RE #170891-0000
Site Address: West 6th and Jasmine Streets
Atlantic Beach, Duval County, FL
SAMPLE
SOIL VAPOR SCREENING RESULTS
BORING
DATE
DEPTH TO
SAMPLE
OVA
NO.
COLLECTED
WATER
DEPTH
READING
COMMENTS
(fbls)
(fbls)
(ppm)
2.0
--------------
0
--------------
---------------------------------------------------
SB-1
2/28/15
3.5
-----4=0-------------
0 ------
--------------------------------------------------
6.0
0
10.0
0
2.0
0
SB -2
2/28/15
3.5
-----4=0-------------
0 ------
--------------------------------------------------
6.0
0
10.0
0
2.0
--------------
0
-------------
---------------------------------------------------
SB-3
2/28/15
3.5
-----4=0-------------
0 ------
---------------------------------------------------
6.0
--------------
0
--------------
---------------------------------------------------
10.0
0.3
-----=-------------
- 0 ------
-------
------------------Lab Sample------------------
SB-4
2/28/15
3.0
-----4=0-------------
-----
-----------------------------------------------------------
- ---------------
---------------------------------- -
6.0
6.0
0
10.0
0
2.0
--------------
0
--------------
--------------------------------------------------
SB-5
2/28/15
3.0
-----4=0-------------
0 ------
--------------------------------------------------
6.0
0
10.0
0
ppm = parts per million
fbls = feet below land surface
OVA = organic vapor analyzer
NM = mot measured
150204—Hancock Bank Proprerty_Tables Page 1 of 7
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APPENDICES
Appendix A
Soil Boring Logs
florida Deparbri m of Fuvit'mucgt rl Pramiitrn - Division of Wagtc Iaf iv%erucrrt - B=au of Netroleum Storage Systoms
BORING LOG
Yana I of
Borin#Well Number:
Permit Number; FDEI' Vacility Idcadfl Sion Number;
sac Name:
Borrhole Start Dato; _ _� Tiorchole Start Time:
AM T— Phi
PARCEL 9170891.0000
E.nd Daie: End Time,
r A -M r PM :
Envirollt metal Contro-utox;
C700100st's Name- Environmental Technician's Nance:
Pfahlar Environment Seivlces, Eno.
R_ Pfahler
R, Pfahler
Drilling Cow"ny: V'x ernwt Thickness (inehes), Borehole Diameter (inches);Borohole Depth (feet):
PROBE DOMAIN
NA 2 -IQ
)hllfing >tdethnd(s): Avpmv Flnreholc D'[1kr Gn feet [vfewurcd Wetl DTW (in W vier JOVA (list model and check type);
5 1wetcr
DIFF teem SDil moistruc
aurttentj:
r rrc�hagP& in well); MinlRse
30M MD fad PID
Di."Mdon ofThill 0ainp [check niethod(s)}:
f Drum I Spnm1 11K fiEE jam" Stockpile Dthc
{rA�scribe if olher or wultyle items ars; Owc1ea1_
Borehole Carnpletion (chcc k one)r, Well
r Gtout r Bmumite Backlil.l r
Other (deacribc)
a r.
.grab Soil wed
Groundwater
; ariple [description
Samples uAt
,7roD p. oy
a
d
y
r (iuckde grain slice �tsed on OWN, rd'ore, staid t$, end w ea aomple PaRtfier
ut➢er renurUg) 3 P
m
and depth or
g ..
Fr
�
� teruporarJ,y¢reeu
D
3
C�
4
�T�.t.,:
l..r.l T..
uauntr+cu Yya; ."AoX rn -mast rxule: n,w = n:�u Altf!�r; S:i S`t' - 3heJby Tube; DF = Diru-t Penh; St:' — Sronic Cory; It'(: = l.ki!! C:uttirtE�
Moisture Cr�nteill CORk ; U = 1)ry; M -� Mo;<q; w = �v� = 5 - r
Florida T)cpmtaimt of Envirtmmtnlal Frosction -Division of waste Manageraent - f3ure= of petroleum Storaip? SyIierrs
13ORING LOG
Page t of
—L—
tirlsigt`ell Nwmber:
PCIMA Plmulxr: FDEF facility Fdentifrtaliun 1,gW11h[S:
sitrl-Name.
Boretrole Stmt Doh.: 24 Anrdl ole Start Time: AM P -M:
PARCEL #170809-90M
Eud Fate. ya- -f� Fad Time, fi Alri
Fnvitvnrncrital co;i rwtar. eologist's Na=; a✓nvirourtientd TechlfidaR'S'4 wale
if
PEahler EnvirartmeriMl Services, In R. P#ahler R. Mahler
1xiAing Company- Pavement Thieknms (inches): .8oreholc D itEntieter (inches). Rolrebole Depth (feet)
PROBE DOMAIN PIA 1 2-1/2
Drilhbg Mathod(s):P:trent Eurehole TJTW (a irat Measured 1[1e11 DTW (in feet aft:r OVA (lis! mral9el and ,.;deck Cts);
DPT S am sail maisWM contend); i �retcr re 9rges in VAI);11AirtiPtae 3aC�E1 Pfl� ++ Plii
171sP43sitl0n of Dell Cuttiq� fcbzL-k mahod(s)). r DTtwi r qpr=d BULkfill s'. , Stockpile Othrr
(describe if alltor or mW p?e irens ore chee-ked),
Bon -hole ComC,le€iari (che� lc ane)f� Vrell i ~ 4rour Bentonhe Bat�Fil� �" Och' ,er (descmbe)
yy� Lab Soil and
on r ip a �7
Groundwaterti
Sample I,�&SCT L10IL
3 P lP F samples (fit
9dIDQd.S m]�Cl'
O :d FF s '�. a D S (fadnde kiln Am bawd Pa USCS, odors, £(3ixJP9, end ell
4�„ g affier rem+rts) and dep.h ur
o S s i � � tenlpur'at',�'screen
u
2
3
4
5
�J
6
.71
IL
,4:�
W d-
F
Z�a{npie 1}'pe L,0aP,5: Mf = YrM Hole; f3A = k11hZa Atr_-Er: NN- 'SY = Shelby Tube,
t_'DP"—!}irCGt �ilaii; Vit= � GuhiC Core: ft t~= tar131 ['tlthYi�S
AM'Wre.3A=DtC=r4E_q: D -Dry' M=Mnist; W-Wel~ S=
Florida Tkpartm mt of Environme�l Protection - Division Of Wage Mmagernertf - Birmna of Pctmltum Storage SrSlerw
BORING LOG
Pete 1 of<
l lot 6ewe'll i` uffiben
permit NwatiKfr
FDEP Facility r(knocatI,oa xknber:
Site Name:
Borehole Start pate, •} Eoubole Start Tim- r• , .,u4 T- PM
d-.
PARCEL *17(l I-OOW
Fed DAte: ,� s� Prld 15ene: r, Am
k'n-wiroamealat CA)n raator:
Geologjst's Name:Bnvi tunentai Fe�altzucian's TVaute;
Pfahlar Environmental Serviop—s, Inc-
R. Pfahler R. Pfahler
D'014w Company: Paverrieu!'li1 d-fless (irlchts): Borehole Diameter (inches): &uobole T)c-Fnh (feet):
PROBE DOMAIN
NA
2-41'd
Nilirg Method(s): lAwirerrt Rmbale DTV? (in feet M�isl�red R+eli Z]� (in feet atter OVA (Fitt mndel and check is pe):
DP7 from spit ntoistum conu,u}: f
, R'sierfa�lbayges iu nKll): NEirtlRlae 30M Fir) 17 piD
fAsposition of llriil Cuffings [check rn lyod(s)):
Druin i—' rcad .131:ickFil] "" 6t ,ckpile Othca
(ifeieribe rf v1h�r c� �rt:elrrpfe il'rrls urti c f ke 1:
thiole Gornflfeiioa (cheek one) r Well r Grout i� BMtou3teX, Uackfift Ofher(describe)
Lob Sail and
pr
rr
Gratesxdwater
Sample Description ��, � gist
Samples s�
p
(inclado Grain size basso on UStl% o&n, stitning, and rr
'!7'S� •� J w
S
�.
6Yier i'l�Yi9YZvT >s'¢' G vad dkpfh or
m u sE
temporary sc.vftn
TY><
2
�•`
J �
j
�.4jt � ��p�
7
n
o
jj1.ry
&4t"-?-AA
f/ fJ
T
-
/f
JY" •.,t^'•.•. i ■.a nr�� rn; �q sui rwj'u Kugrr, a5 S l = :ih:1bP -1 Ube: jlY = }?1rCCt 1�j1{` .�'�'. � 5p111C �U7ci �' h t7iYli1 liitr[n�%
nae�c;lum C.critcnt Crad�s: h _ U«: Ad = Muis� Fr' - iifct; 5 = 'ah d
!'lurid Dcpeztu nt of n►ir�nr„c❑fal Pc+ate,�ion- Division of Waste Management • Bureau Of petroigum Swrne, SYMM
BORING LOG
page l of
1 odugNIell Number
Permit Flumsber:
FDEF Facility Wniifauiari Nurnber:
�
r
site Name;
Errehote SEuf Ilfikc: : % l3or601e Star[ Time: E AM PM
PARCEL #170801-4000
End nate~ End Tina: tit�i r` QM
Jenvirortreental CoiftCu%ir:
Geologist's Name-
Technician's Name;
F%hler Envirorrmerrtal SeMces. Enc.
K. f7Nhlar
R. Mahler
Dii4ing Cwppanp: Fav mens `rhidnm (inches)_ Borehole Dianeut (inches):
&W hole Npth (feet):
I
PROSE DOMAlhd
NA 2-112
- - M )0—
Chilling Wtharf(s):
App went Bnrebde.D71W {in feel
1 egplred Well DIV (iii %eE after
—, .
CiVA (list model and eheCk I3Tc).
DPT
from sail rnoi�iftm caatmt):
hllniRee 30(0 ;� FTD P PID
Disposition of Drill Cuttings jchacic mctitad(s)]:
br pjzu Spread BpdcFikt
�” Sror]tpile other
(de,Feribe if oelrer Or multiple jYems m'e ctucW).-
ireh❑lr Cortrpletiarc fchrCk one} Welk
i Givvt Beatonite Odvx (desojibe)
Lab soil artd
SRnlple Eleseript�n�l
Groundwater
zr n f°• �!
r
a SRmFles {lkst
(ingludt Kn1w size base On Ust 5, vdprs, maiakog, and u S3l0[)}t )1umbeT
atber is Cl
41
r¢murlrs)
soca dcptb err
L
tanpararg scumn
;ut,Y'eal
z
rz'ti'f
r
3
4
•
i1..
�f
r
6
y
G C&
F;
9
1
In
Sa-mpk `)pe [ o&;: PH = Yost }tale: HA = Himd Anger_ S48- 6f, SI - S}xr16r iO,Le: 1)? = Dirv-t Push; SL. — Sunic Ccrc: i3C = fl,ilI Clrttin+ts
AicutureConrcntCodea: D=Dry, V Moisr, W=Wct; R 3;dtva1F4
Flailda Deprfftwnt of Enviraart ulal Prot" -tion - Uivisien of Wasoe Minagrmmt - Bure m of Fleuole= SwAge S`eVzms
BORING LOG
Boring1W01Nuin"f
PerntitNtznlbar: FDEPF�tcilEt� Idea€.i3ic aonNum r:
Sete Mimc;
Borehole. Statt D,4,c,RorEitnle Sf tst Time:
f F
PARCEL #170801-QOW
E.ndDair: .. $ w '~ End Time: AHS FM
-6roamenwl t mtractor
Name: Nane:
PfaNer rEnvirunmMat Servk�FA, tn:
R, PNhler R. PkLh[er
TMIN% compainy:
PsvZmimt'Tbidness (inches)'
Bomb* Dimeter (inchc&)-
P.oreboir, Dopth Yw):
PROBE DOMAIN
NA
2-112
1]rill1118Nfettod(9):
MmvmM Well DSV1(in f6i Oter
OITA (lixL rna&] sad chc0 0 -pe.)-
DPT
&M iotl ruo!Alim caatwt):
wafer rc as s in Kell}:
MiniFk.e 30M HD W 1`11)
DLVositt{1n ofDrtll (,Wings ]chuck meirho;i(s)]: L'ti um Sp ttmd . J l Daobfiif j Ssa lcpik ! OLfix
(describe Vailwr or A211lnpk itc-nu are ch Rd)
]3urelsolc Cotri¢leiion (clteCk irne)', . Wetl Grout Beaioaite lam x. -till Chha (dl's+rijbe)
s,
F.ab SoU rind
.n
rt
Sample Description
�„
=
Groundwater
Sarugles Efist
M_,
t
O
(toclude graf l size based ou EJSCS, vdom �+ai- ing, and
+
ssm¢ie nueai er
_
sfiller
remark;)
3
a
and depth or
o
2rR
"
Fi
�
ttneporarf screen
jpterva]
3
d
€
r
6
?,�
i [l
aempr i ype �c azs; l t7 = r.^st r�nie.; HA �113n0 A4j ¢[; S} _bT = Sbetb,-Tfft; DY —amu F ash-, 9C = Sonic rase; DC - Lirifi Culhrl
Tvfuistwe Contcnt C*dc3; .O — Drr M = Moist; NV - Wel; $ _ n
Appendix B
Analytical Laboratory Report
Aff Hdvanced
Environmental Laboratories, Inc.
March 10, 2015
Randy Pfahler
Pfahler Environmental Services
1212 Forest Oaks Dr
Neptune Beach, FL 32266
RE: Workorder: J1501847 Hancock Bank Property
Dear Randy Pfahler:
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Enclosed are the analytical results for sample(s) received by the laboratory on Monday, March 02, 2015. Results reported herein conform
to the most current NELAC standards, where applicable, unless otherwise narrated in the body of the report. The analytical results for the
samples contained in this report were submitted for analysis as outlined by the Chain of Custody and results pertain only to these samples.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
raw4lft4aakl
Paul Gunsaulies
PGunsaulies@AELLab.com
Enclosures
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
Page 1 of 20
3004.1.0.0
— Hdvaoced
Environmental laboratories, Inc.
SAMPLE SUMMARY
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Workorder: J1501847 Hancock Bank Property
Lab ID Sample ID Matrix Date Collected Date Received
J1501847001 GW -1 Water 2/28/2015 13:45 3/2/2015 08:54
J1501847002 SB -4 Soil 2/28/2015 14:05 3/2/2015 08:54
Report ID: 357001 - 5175626 Page 2 of 20
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
CCOHOY
3004.1.0.0
flduaoced
_ Eovironmental laboratories, Inc.
Workorder: J1501847 Hancock Bank Property
Lab ID: J1501847001
Sample ID: GW -1
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
ANALYTICAL RESULTS
Date Received: 03/02/15 08:54 Matrix: Water
Date Collected: 02/28/15 13:45
Sample Description:
Location:
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
METALS
Analysis Desc: SW846 6010B
Preparation Method: SW -846 3010A
Analysis,Water
Analytical
Method: SW -846 6010
Antimony
0.0060
U
mg/L
1
0.030
0.0060
3/4/201513:41
J
Arsenic
0.0085
U
mg/L
1
0.010
0.0085
3/4/201513:41
J
Beryllium
0.00080
mg/L
1
0.00030
0.00013
3/4/201513:41
J
Cadmium
0.00032
U
mg/L
1
0.00060
0.00032
3/4/201513:41
J
Chromium
0.017
mg/L
1
0.0010
0.00050
3/4/201513:41
J
Copper
0.0025
U
mg/L
1
0.0040
0.0025
3/4/201513:41
J
Lead
0.011
mg/L
1
0.0070
0.0013
3/4/201513:41
J
Nickel
0.0029
1
mg/L
1
0.0065
0.0011
3/4/201513:41
J
Selenium
0.0068
U
mg/L
1
0.020
0.0068
3/4/201513:41
J
Silver
0.0015
1
mg/L
1
0.0040
0.00044
3/4/201513:41
J
Thallium
0.0055
U
mg/L
1
0.025
0.0055
3/4/201513:41
J
Zinc
0.035
mg/L
1
0.010
0.0020
3/4/201513:41
J
Analysis Desc: SW846 7470A
Preparation Method: SW -846 7470A
Analysis,Water
Analytical
Method: SW -846 7470A
Mercury
0.000063
1
mg/L
1
0.00010
0.000010
3/9/201513:29
J
SEMIVOLATILES
Analysis Desc: 8270CAnalysis, Water
Preparation Method: SW -846 3510C
Analytical
Method: SW -846 8270C
1,2,4-Trichlorobenzene
0.69
U
ug/L
1
5.0
0.69
3/6/2015 21:42
J
1,2 -Dichlorobenzene
1.4
U
ug/L
1
5.0
1.4
3/6/2015 21:42
J
1,2-Diphenylhydrazine
0.96
U
ug/L
1
5.0
0.96
3/6/2015 21:42
J
1,3 -Dichlorobenzene
1.0
U
ug/L
1
5.0
1.0
3/6/2015 21:42
J
1,4 -Dichlorobenzene
1.2
U
ug/L
1
5.0
1.2
3/6/2015 21:42
J
2,4,6 -Trichlorophenol
0.93
U
ug/L
1
5.0
0.93
3/6/2015 21:42
J
2,4-Dichlorophenol
0.90
U
ug/L
1
5.0
0.90
3/6/2015 21:42
J
2,4 -Dimethylphenol
2.6
U
ug/L
1
5.0
2.6
3/6/2015 21:42
J
2,4-Dinitrophenol
0.62
U
ug/L
1
10
0.62
3/6/2015 21:42
J
2,4-Dinitrotoluene (2,4-DNT)
0.60
U
ug/L
1
5.0
0.60
3/6/2015 21:42
J
2,6-Dinitrotoluene (2,6-DNT)
1.1
U
ug/L
1
5.0
1.1
3/6/2015 21:42
J
2-Chloronaphthalene
0.97
U
ug/L
1
5.0
0.97
3/6/2015 21:42
J
2 -Chlorophenol
1.2
U
ug/L
1
5.0
1.2
3/6/2015 21:42
J
2-Methyl-4,6-dinitrophenol
0.77
U
ug/L
1
5.0
0.77
3/6/2015 21:42
J
2-Nitrophenol
0.63
U
ug/L
1
5.0
0.63
3/6/2015 21:42
J
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
oH
14 c
ti I h
Page 3 of 20
3004.1.0.0
(a)Advanced
Environmental laboratories, Inc.
ANALYTICAL RESULTS
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Workorder: A501847 Hancock Bank Property
Lab ID: J1501847001
Date Received:
03/02/15 08:54
Matrix:
Water
Sample ID: GW -1
Date Collected:
02/28/15 13:45
Sample Description:
Location:
Adjusted
Adjusted
Parameters Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
3,3'-Dichlorobenzidine
1.3
U
ug/L
1
5.0
1.3
3/6/2015 21:42
J
4-Bromophenyl Phenyl Ether
1.1
U
ug/L
1
5.0
1.1
3/6/2015 21:42
J
4-Chloro-3-methylphenol
0.62
U
ug/L
1
5.0
0.62
3/6/2015 21:42
J
4-Chlorophenyl Phenyl Ether
0.69
U
ug/L
1
5.0
0.69
3/6/2015 21:42
J
4-Nitrophenol
0.62
U
ug/L
1
5.0
0.62
3/6/2015 21:42
J
Acenaphthene
0.96
U
ug/L
1
5.0
0.96
3/6/2015 21:42
J
Acenaphthylene
0.84
U
ug/L
1
5.0
0.84
3/6/2015 21:42
J
Anthracene
0.50
U
ug/L
1
5.0
0.50
3/6/2015 21:42
J
Benzidine
0.74
U
ug/L
1
5.0
0.74
3/6/2015 21:42
J
Benzo[a]anthracene
0.54
U
ug/L
1
5.0
0.54
3/6/2015 21:42
J
Benzo[a]pyrene
0.58
U
ug/L
1
5.0
0.58
3/6/2015 21:42
J
Benzo[b]fluoranthene
0.77
U
ug/L
1
5.0
0.77
3/6/2015 21:42
J
Benzo[g,h,i]perylene
0.76
U
ug/L
1
5.0
0.76
3/6/2015 21:42
J
Benzo[k]fluoranthene
0.70
U
ug/L
1
5.0
0.70
3/6/2015 21:42
J
Butyl benzyl phthalate
1.1
U
ug/L
1
5.0
1.1
3/6/2015 21:42
J
Chrysene
0.67
U
ug/L
1
5.0
0.67
3/6/2015 21:42
J
Di -n -Butyl Phthalate
0.88
U
ug/L
1
5.0
0.88
3/6/2015 21:42
J
Di-n-octyl Phthalate
1.2
U
ug/L
1
5.0
1.2
3/6/2015 21:42
J
Dibenzo[a,h]anthracene
0.73
U
ug/L
1
5.0
0.73
3/6/2015 21:42
J
Diethyl phthalate
0.98
U
ug/L
1
5.0
0.98
3/6/2015 21:42
J
Dimethyl phthalate
1.4
U
ug/L
1
5.0
1.4
3/6/2015 21:42
J
Fluoranthene
0.64
U
ug/L
1
5.0
0.64
3/6/2015 21:42
J
Fluorene
0.85
U
ug/L
1
5.0
0.85
3/6/2015 21:42
J
Hexachlorobenzene
0.99
U
ug/L
1
5.0
0.99
3/6/2015 21:42
J
Hexachlorobutadiene
0.87
U
ug/L
1
5.0
0.87
3/6/2015 21:42
J
Hexachlorocyclopentadiene
0.99
U
ug/L
1
5.0
0.99
3/6/2015 21:42
J
Hexachloroethane
1.2
U
ug/L
1
5.0
1.2
3/6/2015 21:42
J
Indeno(1,2,3-cd)pyrene
0.68
U
ug/L
1
5.0
0.68
3/6/201521:42
J
Isophorone
1.1
U
ug/L
1
5.0
1.1
3/6/2015 21:42
J
N-Nitrosodi-n-propylamine
2.2
U
ug/L
1
5.0
2.2
3/6/2015 21:42
J
N-Nitrosodimethylamine
0.62
U
ug/L
1
5.0
0.62
3/6/2015 21:42
J
N-Nitrosodiphenylamine
0.59
U
ug/L
1
5.0
0.59
3/6/2015 21:42
J
Naphthalene
1.2
U
ug/L
1
5.0
1.2
3/6/2015 21:42
J
Nitrobenzene
1.1
U
ug/L
1
5.0
1.1
3/6/2015 21:42
J
Pentachlorophenol
0.95
U
ug/L
1
5.0
0.95
3/6/2015 21:42
J
Phenanthrene
0.55
U
ug/L
1
5.0
0.55
3/6/2015 21:42
J
Phenol
0.54
U
ug/L
1
5.0
0.54
3/6/2015 21:42
J
Pyrene
0.59
U
ug/L
1
5.0
0.59
3/6/2015 21:42
J
bis(2-Chloroethoxy)methane
1.2
U
ug/L
1
5.0
1.2
3/6/2015 21:42
J
bis(2-Chloroethyl)Ether
1.5
U
ug/L
1
5.0
1.5
3/6/2015 21:42
J
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
= o
~�
U� 4
Page 4 of 20
3004.1.0.0
Hdvanced
- Environmental laboratories, Inc.
ANALYTICAL RESULTS
Workorder: J1501847 Hancock Bank Property
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Lab ID: J1501847001
Sample ID: GW -1
Sample Description:
Date Received:
Date Collected:
Location:
03/02/15 08:54
02/28/15 13:45
Matrix:
Water
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
bis(2-Chloroisopropyl) Ether
1.4
U
ug/L
1
5.0
1.4
3/6/2015 21:42
J
bis(2-Ethylhexyl) phthalate
1.4
U
ug/L
1
5.0
1.4
3/6/2015 21:42
J
2-Fluorophenol (S)
58
%
1
10-90
3/6/2015 21:42
Phenol-d6(S)
43
%
1
10-67
3/6/2015 21:42
Nitrobenzene -d5 (S)
103
%
1
32-147
3/6/2015 21:42
2-Fluorobiphenyl (S)
81
%
1
34-140
3/6/2015 21:42
2,4,6-Tribromophenol (S)
89
%
1
19-190
3/6/2015 21:42
p-Terphenyl-d14 (S)
93
%
1
54-138
3/6/2015 21:42
VOLATILES
Analysis Desc: 8260B Analysis, Water
Preparation Method: SW
-846 5030B
Analytical
Method: SW -846 8260B
1,1,1 -Trichloroethane
0.22
U
ug/L
1
1.0
0.22
3/3/2015 21:13
J
1,1,2,2 -Tetrachloroethane
0.20
U
ug/L
1
1.0
0.20
3/3/2015 21:13
J
1,1,2 -Trichloroethane
0.30
U
ug/L
1
1.0
0.30
3/3/2015 21:13
J
1,1-Dichloroethane
0.14
U
ug/L
1
1.0
0.14
3/3/2015 21:13
J
1,1-Dichloroethylene
0.18
U
ug/L
1
1.0
0.18
3/3/2015 21:13
J
1,2 -Dichlorobenzene
0.18
U
ug/L
1
1.0
0.18
3/3/2015 21:13
J
1,2-Dichloroethane
0.23
U
ug/L
1
1.0
0.23
3/3/2015 21:13
J
1,2-Dichloropropane
0.20
U
ug/L
1
1.0
0.20
3/3/2015 21:13
J
1,3 -Dichlorobenzene
0.19
U
ug/L
1
1.0
0.19
3/3/2015 21:13
J
1,4 -Dichlorobenzene
1.1
ug/L
1
1.0
0.22
3/3/201521:13
J
2-Chloroethyl Vinyl Ether
0.20
U
ug/L
1
5.0
0.20
3/3/2015 21:13
J
Acrolein (Propenal)
1.2
U
ug/L
1
5.0
1.2
3/3/2015 21:13
J
Acrylonitrile
1.1
U
ug/L
1
5.0
1.1
3/3/2015 21:13
J
Benzene
0.21
U
ug/L
1
1.0
0.21
3/3/2015 21:13
J
Bromodichloromethane
0.25
U
ug/L
1
1.0
0.25
3/3/2015 21:13
J
Bromoform
0.43
U
ug/L
1
5.0
0.43
3/3/2015 21:13
J
Bromomethane
0.24
U
ug/L
1
1.0
0.24
3/3/2015 21:13
J
Carbon Tetrachloride
0.36
U
ug/L
1
1.0
0.36
3/3/2015 21:13
J
Chlorobenzene
6.0
ug/L
1
1.0
0.21
3/3/2015 21:13
J
Chloroethane
0.33
U
ug/L
1
1.0
0.33
3/3/2015 21:13
J
Chloroform
0.18
U
ug/L
1
1.0
0.18
3/3/2015 21:13
J
Chloromethane
0.21
U
ug/L
1
1.0
0.21
3/3/2015 21:13
J
Dibromochloromethane
0.33
U
ug/L
1
1.0
0.33
3/3/2015 21:13
J
Dichlorodifluoromethane
0.15
U
ug/L
1
1.0
0.15
3/3/2015 21:13
J
Ethylbenzene
0.24
U
ug/L
1
1.0
0.24
3/3/2015 21:13
J
Methylene Chloride
1.0
U
ug/L
1
5.0
1.0
3/3/2015 21:13
J
Tetrachloroethylene (PCE)
0.36
U
ug/L
1
1.0
0.36
3/3/2015 21:13
J
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
Page 5 of 20
3004.1.0.0
Aff- - flduaoced
Environmental laboratories, Inc.
ANALYTICAL RESULTS
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Workorder: J1501847 Hancock Bank Property
Lab ID: J1501847001
Date Received:
03/02/15 08:54
Matrix:
Water
Sample ID: GW -1
Date Collected:
02/28/15 13:45
Sample Description:
Location:
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
Toluene
0.23
U
ug/L
1
1.0
0.23
3/3/2015 21:13
J
Trichloroethene
0.29
U
ug/L
1
1.0
0.29
3/3/2015 21:13
J
Trichlorofluoromethane
0.32
U
ug/L
1
1.0
0.32
3/3/2015 21:13
J
Vinyl Chloride
0.24
U
ug/L
1
1.0
0.24
3/3/2015 21:13
J
Xylene (Total)
0.53
U
ug/L
1
3.0
0.53
3/3/2015 21:13
J
cis-1,2-Dichloroethylene
0.24
U
ug/L
1
1.0
0.24
3/3/2015 21:13
J
cis-1,3-Dichloropropene
0.16
U
ug/L
1
1.0
0.16
3/3/2015 21:13
J
trans- 1,2-D ichloroethylene
0.20
U
ug/L
1
1.0
0.20
3/3/2015 21:13
J
trans- 1,3-D ichloropropylene
0.18
U
ug/L
1
5.0
0.18
3/3/2015 21:13
J
1,2-Dichloroethane-d4 (S)
97
%
1
80-120
3/3/2015 21:13
Toluene -d8 (S)
104
%
1
88-110
3/3/2015 21:13
Bromofluorobenzene (S)
102
%
1
86-115
3/3/2015 21:13
Lab ID: J1501847002
Date Received:
03/02/15 08:54
Matrix:
Soil
Sample ID: SB -4
Date Collected:
02/28/15 14:05
Results for sample A 501847002 are
reported on a dry weight basis.
Sample Description:
Location:
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
METALS
Analysis Desc: SW846 6010B
Preparation Method: SW -846 3050B
Analysis,Soils
Analytical
Method: SW -846 6010
Antimony
0.14
U
mg/Kg
1
0.85
0.14
3/5/2015 00:18
J
Arsenic
0.26
U
mg/Kg
1
0.28
0.26
3/5/2015 00:18
J
Beryllium
0.058
mg/Kg
1
0.0085
0.0024
3/5/2015 00:18
J
Cadmium
0.14
1
mg/Kg
1
0.17
0.036
3/5/2015 00:18
J
Chromium
2.9
mg/Kg
1
0.11
0.067
3/5/2015 00:18
J
Copper
35
mg/Kg
1
0.11
0.061
3/5/2015 00:18
J
Lead
5.5
mg/Kg
1
0.20
0.057
3/5/2015 00:18
J
Nickel
2.1
mg/Kg
1
0.18
0.055
3/5/2015 00:18
J
Selenium
0.21
U
mg/Kg
1
0.57
0.21
3/5/2015 00:18
J
Silver
0.034
U
mg/Kg
1
0.11
0.034
3/5/2015 00:18
J
Thallium
0.15
U
mg/Kg
1
0.71
0.15
3/5/2015 00:18
J
Zinc
35
mg/Kg
1
0.28
0.21
3/5/2015 00:18
J
Report ID: 357001 - 5175626 Page 6 of 20
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
r Op�Y
3004.1.0.0
flduanced
Environmental Laboratories, Inc.
ANALYTICAL RESULTS
Workorder: J1501847 Hancock Bank Property
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Lab ID: J1501847002
Sample ID: SB -4
Results for sample J1501847002 are reported on a dry weight basis.
Sample Description:
Date Received:
Date Collected:
Location:
03/02/15 08:54
02/28/15 14:05
Matrix:
Soil
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
Analysis Desc: SW846 7471AAnalysis,
Preparation Method: SW -846 7471A
Soil
Analytical
Method: SW -846
7471A
Mercury
0.023
mg/Kg
1
0.0052
0.00073
3/6/201511:34
J
SEMIVOLATILES
Analysis Desc: 8270C Analysis, Soil
Preparation Method: SW -846 3550B
Analytical
Method: SW -846 8270C
1,2,4-Trichlorobenzene
0.026
U
mg/Kg
1
0.20
0.026
3/7/201504:45
J
1,2 -Dichlorobenzene
0.028
U
mg/Kg
1
0.20
0.028
3/7/2015 04:45
J
1,2-Diphenylhydrazine
0.016
U
mg/Kg
1
0.20
0.016
3/7/2015 04:45
J
1,3 -Dichlorobenzene
0.024
U
mg/Kg
1
0.20
0.024
3/7/2015 04:45
J
1,4 -Dichlorobenzene
0.030
U
mg/Kg
1
0.20
0.030
3/7/2015 04:45
J
2,4,6 -Trichlorophenol
0.022
U
mg/Kg
1
0.20
0.022
3/7/2015 04:45
J
2,4-Dichlorophenol
0.026
U
mg/Kg
1
0.20
0.026
3/7/2015 04:45
J
2,4 -Dimethylphenol
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
2,4-Dinitrophenol
0.065
U
mg/Kg
1
0.40
0.065
3/9/201519:31
J
2,4-Dinitrotoluene (2,4-DNT)
0.022
U
mg/Kg
1
0.20
0.022
3/7/2015 04:45
J
2,6-Dinitrotoluene (2,6-DNT)
0.032
U
mg/Kg
1
0.20
0.032
3/7/2015 04:45
J
2-Chloronaphthalene
0.021
U
mg/Kg
1
0.20
0.021
3/7/2015 04:45
J
2 -Chlorophenol
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
2-Methyl-4,6-dinitrophenol
0.044
U
mg/Kg
1
0.20
0.044
3/7/2015 04:45
J
2-Nitrophenol
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
3,3'-Dichlorobenzidine
0.030
U
mg/Kg
1
0.20
0.030
3/7/2015 04:45
J
4-Bromophenyl Phenyl Ether
0.027
U
mg/Kg
1
0.20
0.027
3/7/2015 04:45
J
4-Chloro-3-methylphenol
0.016
U
mg/Kg
1
0.20
0.016
3/7/2015 04:45
J
4-Chlorophenyl Phenyl Ether
0.030
U
mg/Kg
1
0.20
0.030
3/7/2015 04:45
J
4-Nitrophenol
0.049
U
mg/Kg
1
0.20
0.049
3/7/2015 04:45
J
Acenaphthene
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
Acenaphthylene
0.015
U
mg/Kg
1
0.20
0.015
3/7/2015 04:45
J
Anthracene
0.017
U
mg/Kg
1
0.20
0.017
3/7/2015 04:45
J
Benzidine
0.014
U
mg/Kg
1
0.20
0.014
3/7/2015 04:45
J
Benzo[a]anthracene
0.017
U
mg/Kg
1
0.20
0.017
3/7/2015 04:45
J
Benzo[a]pyrene
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
Benzo[b]fluoranthene
0.016
U
mg/Kg
1
0.20
0.016
3/7/2015 04:45
J
Benzo[g,h,i]perylene
0.022
U
mg/Kg
1
0.20
0.022
3/7/2015 04:45
J
Benzo[k]fluoranthene
0.020
U
mg/Kg
1
0.20
0.020
3/7/2015 04:45
J
Butyl benzyl phthalate
0.020
U
mg/Kg
1
0.20
0.020
3/7/2015 04:45
J
Chrysene
0.017
U
mg/Kg
1
0.20
0.017
3/7/2015 04:45
J
Di -n -Butyl Phthalate
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
��ogoy
Page 7 of 20
3004.1.0.0
�- - flduanced
Environmental [aboratories, Inc.
ANALYTICAL RESULTS
Workorder: J1501847 Hancock Bank Property
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Lab ID: J1501847002
Sample ID: SB4
Results for sample J1501847002 are reported on a dryweight basis.
Sample Description:
Date Received:
Date Collected:
Location:
03/02/15 08:54
02/28/15 14:05
Matrix:
Soil
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
Di-n-octyl Phthalate
0.030
U
mg/Kg
1
0.20
0.030
3/7/2015 04:45
J
Dibenzo[a,h]anthracene
0.021
U
mg/Kg
1
0.20
0.021
3/7/2015 04:45
J
Diethyl phthalate
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
Dimethyl phthalate
0.043
1
mg/Kg
1
0.20
0.024
3/7/2015 04:45
J
Fluoranthene
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
Fluorene
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
Hexachlorobenzene
0.034
U
mg/Kg
1
0.20
0.034
3/7/2015 04:45
J
Hexachlorobutadiene
0.034
U
mg/Kg
1
0.20
0.034
3/7/2015 04:45
J
Hexachlorocyclopentadiene
0.020
U
mg/Kg
1
0.20
0.020
3/7/2015 04:45
J
Hexachloroethane
0.033
U
mg/Kg
1
0.20
0.033
3/7/2015 04:45
J
Indeno(1,2,3-cd)pyrene
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
Isophorone
0.020
U
mg/Kg
1
0.20
0.020
3/7/2015 04:45
J
N-Nitrosodi-n-propylamine
0.015
U
mg/Kg
1
0.20
0.015
3/7/2015 04:45
J
N-Nitrosodimethylamine
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
N-Nitrosodiphenylamine
0.016
U
mg/Kg
1
0.20
0.016
3/7/2015 04:45
J
Naphthalene
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
Nitrobenzene
0.016
U
mg/Kg
1
0.20
0.016
3/7/2015 04:45
J
Pentachlorophenol
0.039
U
mg/Kg
1
0.20
0.039
3/9/201519:31
J
Phenanthrene
0.015
U
mg/Kg
1
0.20
0.015
3/7/2015 04:45
J
Phenol
0.020
U
mg/Kg
1
0.20
0.020
3/7/2015 04:45
J
Pyrene
0.015
U
mg/Kg
1
0.20
0.015
3/7/2015 04:45
J
bis(2-Chloroethoxy)methane
0.019
U
mg/Kg
1
0.20
0.019
3/7/2015 04:45
J
bis(2-Chloroethyl)Ether
0.022
U
mg/Kg
1
0.20
0.022
3/7/2015 04:45
J
bis(2-Chloroisopropyl) Ether
0.018
U
mg/Kg
1
0.20
0.018
3/7/2015 04:45
J
bis(2-Ethylhexyl) phthalate
0.024
U
mg/Kg
1
0.20
0.024
3/7/2015 04:45
J
2-Fluorophenol (S)
80
%
1
59-122
3/7/2015 04:45
Phenol-d6(S)
83
%
1
54-124
3/7/2015 04:45
Nitrobenzene -d5 (S)
84
%
1
46-118
3/7/2015 04:45
2-Fluorobiphenyl (S)
59
%
1
54-134
3/7/2015 04:45
2,4,6-Tribromophenol (S)
87
%
1
38-141
3/7/2015 04:45
p-Terphenyl-dl4 (S)
88
%
1
60-143
3/7/2015 04:45
VOLATILES
Analysis Desc: 8260B Analysis, Soil
Preparation Method: SW -846 5035
Analytical
Method: SW -846 8260B
1,1,1 -Trichloroethane
1.4
U
ug/Kg
1
3.0
1.4
3/3/201515:35
J
1,1,2,2 -Tetrachloroethane
2.0
U
ug/Kg
1
3.0
2.0
3/3/201515:35
J
1,1,2 -Trichloroethane
1.4
U
ug/Kg
1
3.0
1.4
3/3/201515:35
J
1,1-Dichloroethane
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
'= o
�c C Apy
Page 8 of 20
3004.1.0.0
- Maud
Eaviraameatal [ahoratories, Inc.
ANALYTICAL RESULTS
Workorder: J1501847 Hancock Bank Property
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Lab ID: J1501847002
Date Received:
03/02/15 08:54
Matrix:
Soil
Sample ID: SB -4
Date Collected:
02/28/15 14:05
Results for sample J1501847002 are
reported on a dry weight basis.
Sample Description:
Location:
Adjusted
Adjusted
Parameters
Results
Qual
Units
DF
PQL
MDL
Analyzed
Lab
1,1-Dichloroethylene
1.2
U
ug/Kg
1
3.0
1.2
3/3/201515:35
J
1,2 -Dichlorobenzene
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
1,2-Dichloroethane
1.4
U
ug/Kg
1
3.0
1.4
3/3/201515:35
J
1,2-Dichloropropane
1.2
U
ug/Kg
1
3.0
1.2
3/3/201515:35
J
1,3 -Dichlorobenzene
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
1,4 -Dichlorobenzene
1.2
U
ug/Kg
1
3.0
1.2
3/3/201515:35
J
2-Chloroethyl Vinyl Ether
0.77
U
ug/Kg
1
5.0
0.77
3/3/2015 15:35
J
Acrolein (Propenal)
4.1
U
ug/Kg
1
15
4.1
3/3/2015 15:35
J
Acrylonitrile
5.2
U
ug/Kg
1
15
5.2
3/3/201515:35
J
Benzene
1.2
U
ug/Kg
1
3.0
1.2
3/3/201515:35
J
Bromodichloromethane
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
Bromoform
2.0
U
ug/Kg
1
5.0
2.0
3/3/201515:35
J
Bromomethane
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
Carbon Tetrachloride
1.4
U
ug/Kg
1
3.0
1.4
3/3/2015 15:35
J
Chlorobenzene
1.5
U
ug/Kg
1
3.0
1.5
3/3/201515:35
J
Chloroethane
1.0
U
ug/Kg
1
3.0
1.0
3/3/201515:35
J
Chloroform
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
Chloromethane
1.0
U
ug/Kg
1
3.0
1.0
3/3/201515:35
J
Dibromochloromethane
1.3
U
ug/Kg
1
3.0
1.3
3/3/201515:35
J
Dichlorodifluoromethane
0.85
U
ug/Kg
1
3.0
0.85
3/3/201515:35
J
Ethylbenzene
1.1
U
ug/Kg
1
3.0
1.1
3/3/201515:35
J
Methylene Chloride
2.0
1
ug/Kg
1
10
1.2
3/3/2015 15:35
J
Tetrachloroethylene (PCE)
1.2
U
ug/Kg
1
3.0
1.2
3/3/2015 15:35
J
Toluene
1.4
U
ug/Kg
1
3.0
1.4
3/3/201515:35
J
Trichloroethene
1.0
U
ug/Kg
1
3.0
1.0
3/3/201515:35
J
Trichlorofluoromethane
0.92
U
ug/Kg
1
3.0
0.92
3/3/201515:35
J
Vinyl Chloride
1.2
U
ug/Kg
1
3.0
1.2
3/3/2015 15:35
J
Xylene (Total)
3.8
U
ug/Kg
1
9.1
3.8
3/3/2015 15:35
J
cis-1,2-Dichloroethylene
1.4
U
ug/Kg
1
3.0
1.4
3/3/201515:35
J
cis-1,3-Dichloropropene
1.1
U
ug/Kg
1
3.0
1.1
3/3/201515:35
J
trans-1,2-Dichloroethylene
0.99
U
ug/Kg
1
3.0
0.99
3/3/201515:35
J
trans-1,3-Dichloropropylene
0.76
U
ug/Kg
1
3.0
0.76
3/3/201515:35
J
1,2-Dichloroethane-d4 (S)
97
%
1
80-120
3/3/2015 15:35
Toluene -d8 (S)
102
%
1
81-117
3/3/2015 15:35
Bromofluorobenzene (S)
107
%
1
74-121
3/3/2015 15:35
VOLATILES
Analysis Desc: Percent Analytical Method: SM 2540G
Solids,SM2540G,Soil
Percent Moisture 15 % 1 3/2/2015 10:20 J
Report ID: 357001 - 5175626 Page 9 of 20
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PARAMETER QUALIFIERS
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
ANALYTICAL RESULTS QUALIFIERS
The compound was analyzed for but not detected.
Phone: (904)363-9350
Fax: (904)363-9354
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
LAB QUALIFIERS
DOH Certification #E82574(AEL-JAX)(FL NELAC Certification)
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
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QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
QC Batch: DGMj/1208 Analysis Method: SW -846 6010
QC Batch Method: SW -846 3010A Prepared: 03/03/2015 03:30
Associated Lab Samples: J1501847001
METHOD BLANK: 1690262
Blank Reporting
Parameter Units Result Limit Qualifiers
METALS
0.84
0.84 U
ug/Kg
Silver
mg/L
0.00044
0.00044 U
Arsenic
mg/L
0.0085
0.0085 U
Beryllium
mg/L
0.00013
0.00013 U
Cadmium
mg/L
0.00032
0.00032 U
Chromium
mg/L
0.00050
0.00050 U
Copper
mg/L
0.0025
0.0025 U
Nickel
mg/L
0.0011
0.0011 U
Lead
mg/L
0.0013
0.0013 U
Antimony
mg/L
0.0060
0.0060 U
Selenium
mg/L
0.0068
0.0068 U
Thallium
mg/L
0.0055
0.0055 U
Zinc
mg/L
0.0020
0.0020 U
QC Batch: MSVj/1206 Analysis Method:
QC Batch Method: SW -846 5035 Prepared:
Associated Lab Samples: J1501847002
METHOD BLANK: 1690696
Blank Reporting
Parameter Units Result Limit Qualifiers
VOLATILES
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
Acrolein (Propenal)
1,1-Dichloroethylene
Acrylonitrile
Methylene Chloride
trans-1,2-Dichloroethylene
1, 1 -Dich loro ethane
cis-1,2-Dichloroethylene
Chloroform
1,2-Dichloroethane
Report ID: 357001 - 5175626
ug/Kg
0.84
0.84 U
ug/Kg
1.0
1.0 U
ug/Kg
1.2
1.2 U
ug/Kg
1.3
1.3 U
ug/Kg
1.0
1.0 U
ug/Kg
0.91
0.91 U
ug/Kg
4.1
4.1 U
ug/Kg
1.2
1.2 U
ug/Kg
5.2
5.2 U
ug/Kg
1.2
1.2 U
ug/Kg
0.98
0.98 U
ug/Kg
1.3
1.3 U
ug/Kg
1.4
1.4 U
ug/Kg
1.3
1.3 U
ug/Kg
1.4
1.4 U
SW -846 8260B
03/02/2015 09:26
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
� c
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QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
METHOD BLANK: 1690696
Blank Reporting
Parameter Units Result Limit Qualifiers
1,1,1 -Trichloroethane
ug/Kg
1.4
1.4 U
Carbon Tetrachloride
ug/Kg
1.4
1.4 U
Benzene
ug/Kg
1.2
1.2 U
1,2-Dichloropropane
ug/Kg
1.2
1.2 U
Trichloroethene
ug/Kg
1.0
1.0 U
Bromodichloromethane
ug/Kg
1.3
1.3 U
2-Chloroethyl Vinyl Ether
ug/Kg
0.76
0.76 U
cis-1,3-Dichloropropene
ug/Kg
1.1
1.1 U
trans- 1,3-Dichloropropylene
ug/Kg
0.75
0.75 U
1,1,2 -Trichloroethane
ug/Kg
1.3
1.3 U
Toluene
ug/Kg
1.4
1.4 U
Dibromochloromethane
ug/Kg
1.3
1.3 U
Tetrachloroethylene (PCE)
ug/Kg
1.2
1.2 U
Chlorobenzene
ug/Kg
1.4
1.4 U
Ethylbenzene
ug/Kg
1.1
1.1 U
Bromoform
ug/Kg
1.9
1.9 U
1,1,2,2 -Tetrachloroethane
ug/Kg
2.0
2.0 U
1,3 -Dichlorobenzene
ug/Kg
1.3
1.3 U
1,4 -Dichlorobenzene
ug/Kg
1.1
1.1 U
1,2 -Dichlorobenzene
ug/Kg
1.3
1.3 U
Xylene (Total)
ug/Kg
3.8
3.8 U
1,2-Dichloroethane-d4 (S)
%
97
80-120
Toluene -d8 (S)
%
100
81-117
Bromofluorobenzene (S)
%
104
74-121
QC Batch: MSVj/1210 Analysis Method
QC Batch Method: SW -846 5030B Prepared:
Associated Lab Samples: J1501847001
METHOD BLANK: 1691391
Blank Reporting
Parameter Units Result Limit Qualifiers
VOLATILES
Dichlorodifluoromethane
Chloromethane
Vinyl Chloride
Bromomethane
Chloroethane
Trichlorofluoromethane
Acrolein (Propenal)
1,1-Dichloroethylene
Acrylonitrile
Report ID: 357001 - 5175626
ug/L
0.15
0.15 U
ug/L
0.21
0.21 U
ug/L
0.24
0.24 U
ug/L
0.24
0.24 U
ug/L
0.33
0.33 U
ug/L
0.32
0.32 U
ug/L
1.2
1.2 U
ug/L
0.18
0.18 U
ug/L
1.1
1.1 U
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
SW -846 8260B
03/03/2015 09:49
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
Op�N
Page 12 of 20
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Advanced
Environmental laboratories, Inc.
QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
METHOD BLANK: 1691391
Blank Reporting
Parameter Units Result Limit Qualifiers
Methylene Chloride
ug/L
1.0
1.0 U
trans-1,2-Dichloroethylene
ug/L
0.20
0.20 U
1,1-Dichloroethane
ug/L
0.14
0.14 U
cis-1,2-Dichloroethylene
ug/L
0.24
0.24 U
Chloroform
ug/L
0.18
0.18 U
1,2-Dichloroethane
ug/L
0.23
0.23 U
1,1,1 -Trichloroethane
ug/L
0.22
0.22 U
Carbon Tetrachloride
ug/L
0.36
0.36 U
Benzene
ug/L
0.21
0.21 U
1,2-Dichloropropane
ug/L
0.20
0.20 U
Trichloroethene
ug/L
0.29
0.29 U
Bromodichloromethane
ug/L
0.25
0.25 U
2-Chloroethyl Vinyl Ether
ug/L
0.20
0.20 U
cis-1,3-Dichloropropene
ug/L
0.16
0.16 U
trans-1,3-Dichloropropylene
ug/L
0.18
0.18 U
1,1,2 -Trichloroethane
ug/L
0.30
0.30 U
Toluene
ug/L
0.23
0.23 U
Dibromochloromethane
ug/L
0.33
0.33 U
Tetrachloroethylene (PCE)
ug/L
0.36
0.36 U
Chlorobenzene
ug/L
0.21
0.21 U
Ethylbenzene
ug/L
0.24
0.24 U
Bromoform
ug/L
0.43
0.43 U
1,1,2,2 -Tetrachloroethane
ug/L
0.20
0.20 U
1,3 -Dichlorobenzene
ug/L
0.19
0.19 U
1,4 -Dichlorobenzene
ug/L
0.22
0.22 U
1,2 -Dichlorobenzene
ug/L
0.18
0.18 U
Xylene (Total)
ug/L
0.53
0.53 U
1,2-Dichloroethane-d4 (S)
%
112
80-120
Toluene -d8 (S)
%
102
88-110
Bromofluorobenzene (S)
%
105
86-115
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
QC Batch: DGMj/1211
QC Batch Method: SW -846 3050B
Associated Lab Samples: J1501847002
Analysis Method: SW -846 6010
Prepared: 03/04/2015 10:19
METHOD BLANK:
1691932
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
METALS
Silver
mg/Kg
0.0012
0.0012 U
Arsenic
mg/Kg
0.0091
0.0091 U
Beryllium
mg/Kg
0.000086
0.000086 U
Report ID: 357001 -5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
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Page 13 of 20
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QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
METHOD BLANK: 1691932
Blank Reporting
Parameter Units Result Limit Qualifiers
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
Cadmium
mg/Kg
0.0013
0.0013 U
Chromium
mg/Kg
0.0024
0.0024 U
Copper
mg/Kg
0.0022
0.0022 U
Nickel
mg/Kg
0.0019
0.0019 U
Lead
mg/Kg
0.0020
0.0020 U
Selenium
mg/Kg
0.0075
0.0075 U
Thallium
mg/Kg
0.0052
0.0052 U
Zinc
mg/Kg
0.0075
0.0075 U
2,4-Dinitrophenol
mg/Kg
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
METALS
Antimony
mg/Kg 0.0049 0.0049 U
QC Batch: EXTj/1252 Analysis Method: SW -846 8270C
QC Batch Method: SW -846 3550B Prepared: 03/05/2015 09:00
Associated Lab Samples: J1501847002
METHOD BLANK: 1693431
Blank Reporting
Parameter Units Result Limit Qualifiers
SEMIVOLATILES
Phenol
mg/Kg
0.017
0.017 U
2 -Chlorophenol
mg/Kg
0.016
0.016 U
2-Nitrophenol
mg/Kg
0.015
0.015 U
2,4 -Dimethylphenol
mg/Kg
0.016
0.016 U
2,4-Dichlorophenol
mg/Kg
0.022
0.022 U
4-Chloro-3-methylphenol
mg/Kg
0.013
0.013 U
2,4,6 -Trichlorophenol
mg/Kg
0.019
0.019 U
2,4-Dinitrophenol
mg/Kg
0.055
0.055 U
4-Nitrophenol
mg/Kg
0.041
0.041 U
2-Methyl-4,6-dinitrophenol
mg/Kg
0.037
0.037 U
Pentachlorophenol
mg/Kg
0.033
0.033 U
N-Nitrosodimethylamine
mg/Kg
0.016
0.016 U
bis(2-Chloroethyl)Ether
mg/Kg
0.018
0.018 U
1,3 -Dichlorobenzene
mg/Kg
0.021
0.021 U
1,4 -Dichlorobenzene
mg/Kg
0.025
0.025 U
1,2 -Dichlorobenzene
mg/Kg
0.023
0.023 U
bis(2-Chloroisopropyl) Ether
mg/Kg
0.015
0.015 U
N-Nitrosodi-n-propylamine
mg/Kg
0.013
0.013 U
Hexachloroethane
mg/Kg
0.028
0.028 U
Nitrobenzene
mg/Kg
0.013
0.013 U
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
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hvironmental [aboratories, Inc.
QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
METHOD BLANK: 1693431
Blank Reporting
Parameter Units Result Limit Qualifiers
Isophorone
mg/Kg
0.017
0.017 U
bis(2-Chloroethoxy)methane
mg/Kg
0.016
0.016 U
1,2,4-Trichlorobenzene
mg/Kg
0.022
0.022 U
Naphthalene
mg/Kg
0.015
0.015 U
Hexachlorobutadiene
mg/Kg
0.028
0.028 U
Hexachlorocyclopentadiene
mg/Kg
0.017
0.017 U
2-Chloronaphthalene
mg/Kg
0.018
0.018 U
Dimethyl phthalate
mg/Kg
0.021
0.021 U
2,6-Dinitrotoluene (2,6-DNT)
mg/Kg
0.027
0.027 U
Acenaphthylene
mg/Kg
0.013
0.013 U
Acenaphthene
mg/Kg
0.016
0.016 U
2,4-Dinitrotoluene (2,4-DNT)
mg/Kg
0.018
0.018 U
Diethyl phthalate
mg/Kg
0.015
0.015 U
Fluorene
mg/Kg
0.016
0.016 U
4-Chlorophenyl Phenyl Ether
mg/Kg
0.025
0.025 U
1,2-Diphenylhydrazine
mg/Kg
0.013
0.013 U
4-Bromophenyl Phenyl Ether
mg/Kg
0.023
0.023 U
Hexachlorobenzene
mg/Kg
0.028
0.028 U
Phenanthrene
mg/Kg
0.012
0.012 U
Anthracene
mg/Kg
0.014
0.014 U
Di -n -Butyl Phthalate
mg/Kg
0.015
0.015 U
Fluoranthene
mg/Kg
0.016
0.016 U
Benzidine
mg/Kg
0.012
0.012 U
Pyrene
mg/Kg
0.013
0.013 U
Butyl benzyl phthalate
mg/Kg
0.017
0.017 U
Benzo[a]anthracene
mg/Kg
0.014
0.014 U
3,3'-Dichlorobenzidine
mg/Kg
0.025
0.025 U
Chrysene
mg/Kg
0.014
0.014 U
bis(2-Ethylhexyl) phthalate
mg/Kg
0.020
0.020 U
Di-n-octyl Phthalate
mg/Kg
0.025
0.025 U
Benzo[b]fluoranthene
mg/Kg
0.013
0.013 U
Benzo[k]fluoranthene
mg/Kg
0.017
0.017 U
Benzo[a]pyrene
mg/Kg
0.015
0.015 U
Indeno(1,2,3-cd)pyrene
mg/Kg
0.016
0.016 U
Dibenzo[a,h]anthracene
mg/Kg
0.017
0.017 U
Benzo[g,h,i]perylene
mg/Kg
0.018
0.018 U
N-Nitrosodiphenylamine
mg/Kg
0.014
0.014 U
2-Fluorophenol (S)
%
89
59-122
Phenol-d6(S)
%
82
54-124
Nitrobenzene -d5 (S)
%
83
46-118
2-Fluorobiphenyl (S)
%
81
54-134
2,4,6-Tribromophenol (S)
%
72
38-141
p-Terphenyl-d14 (S)
%
85
60-143
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
' SAO
Phone: (904)363-9350
Fax: (904)363-9354
Page 15 of 20
3004.1.0.0
= Hdvanced
Environmental laboratories, Inc.
Workorder: J1501847 Hancock Bank Property
QC Batch: EXTj/1259
QC Batch Method: SW -846 3510C
Associated Lab Samples: J1501847001
METHOD BLANK: 1694631
QUALITY CONTROL DATA
Analysis Method:
Prepared:
Blank Reporting
Parameter Units Result Limit Qualifiers
SEMIVOLATILES
Phenol
ug/L
0.54
0.54 U
2 -Chlorophenol
ug/L
1.2
1.2 U
2-Nitrophenol
ug/L
0.63
0.63 U
2,4 -Dimethylphenol
ug/L
2.6
2.6 U
2,4-Dichlorophenol
ug/L
0.90
0.90 U
4-Chloro-3-methylphenol
ug/L
0.62
0.62 U
2,4,6 -Trichlorophenol
ug/L
0.93
0.93 U
2,4-Dinitrophenol
ug/L
0.62
0.62 U
4-Nitrophenol
ug/L
0.62
0.62 U
2-Methyl-4,6-dinitrophenol
ug/L
0.77
0.77 U
Pentachlorophenol
ug/L
0.95
0.95 U
N-Nitrosodimethylamine
ug/L
0.62
0.62 U
bis(2-Chloroethyl)Ether
ug/L
1.5
1.5 U
1,3 -Dichlorobenzene
ug/L
1.0
1.0 U
1,4 -Dichlorobenzene
ug/L
1.2
1.2 U
1,2 -Dichlorobenzene
ug/L
1.4
1.4 U
bis(2-Chloroisopropyl) Ether
ug/L
1.4
1.4 U
N-Nitrosodi-n-propylamine
ug/L
2.2
2.2 U
Hexachloroethane
ug/L
1.2
1.2 U
Nitrobenzene
ug/L
1.1
1.1 U
Isophorone
ug/L
1.1
1.1 U
bis(2-Chloroethoxy)methane
ug/L
1.2
1.2 U
1,2,4-Trichlorobenzene
ug/L
0.69
0.69 U
Naphthalene
ug/L
1.2
1.2 U
Hexachlorobutadiene
ug/L
0.87
0.87 U
Hexachlorocyclopentadiene
ug/L
0.99
0.99 U
2-Chloronaphthalene
ug/L
0.97
0.97 U
Dimethyl phthalate
ug/L
1.4
1.4 U
2,6-Dinitrotoluene (2,6-DNT)
ug/L
1.1
1.1 U
Acenaphthylene
ug/L
0.84
0.84 U
Acenaphthene
ug/L
0.96
0.96 U
2,4-Dinitrotoluene (2,4-DNT)
ug/L
0.60
0.60 U
Diethyl phthalate
ug/L
0.98
0.98 U
Fluorene
ug/L
0.85
0.85 U
4-Chlorophenyl Phenyl Ether
ug/L
0.69
0.69 U
1,2-Diphenylhydrazine
ug/L
0.96
0.96 U
4-Bromophenyl Phenyl Ether
ug/L
1.1
1.1 U
Hexachlorobenzene
ug/L
0.99
0.99 U
Phenanthrene
ug/L
0.55
0.55 U
Report ID: 357001 - 5175626
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
SW -846 8270C
03/05/2015 17:30
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
Cpg
403&
f
Phone: (904)363-9350
Fax: (904)363-9354
Page 16 of 20
3004.1.0.0
Aff 19
= Advanced
Environmental Laboratories, Inc.
QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
METHOD BLANK: 1694631
Blank Reporting
Parameter Units Result Limit Qualifiers
Anthracene
ug/L
0.50
0.50 U
Di -n -Butyl Phthalate
ug/L
0.88
0.88 U
Fluoranthene
ug/L
0.64
0.64 U
Benzidine
ug/L
0.74
0.74 U
Pyrene
ug/L
0.59
0.59 U
Butyl benzyl phthalate
ug/L
1.1
1.1 U
Benzo[a]anthracene
ug/L
0.54
0.54 U
3,3'-Dichlorobenzidine
ug/L
1.3
1.3 U
Chrysene
ug/L
0.67
0.67 U
bis(2-Ethylhexyl) phthalate
ug/L
1.4
1.4 U
Di-n-octyl Phthalate
ug/L
1.2
1.2 U
Benzo[b]fluoranthene
ug/L
0.77
0.77 U
Benzo[k]fluoranthene
ug/L
0.70
0.70 U
Benzo[a]pyrene
ug/L
0.58
0.58 U
Indeno(1,2,3-cd)pyrene
ug/L
0.68
0.68 U
Dibenzo[a,h]anthracene
ug/L
0.73
0.73 U
Benzo[g,h,i]perylene
ug/L
0.76
0.76 U
N-Nitrosodiphenylamine
ug/L
0.59
0.59 U
2-Fluorophenol (S)
%
62
10-90
Phenol-d6(S)
%
43
10-67
Nitrobenzene -d5 (S)
%
98
32-147
2-Fluorobiphenyl (S)
%
105
34-140
2,4,6-Tribromophenol (S)
%
113
19-190
p-Terphenyl-d14 (S)
%
112
54-138
QC Batch: DGMj/1216
QC Batch Method: SW -846 7471A
Associated Lab Samples: J1501847002
METHOD BLANK: 1694659
Parameter
METALS
Mercury
Units
mg/Kg
QC Batch: DGMj/1237
QC Batch Method: SW -846 7470A
Associated Lab Samples: J1501847001
Report ID: 357001 - 5175626
Analysis Method
Prepared:
Blank Reporting
Result Limit Qualifiers
0.00042 0.00042 U
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
SW -846 7471A
03/06/2015 08:48
Analysis Method: SW -846 7470A
Prepared: 03/09/2015 09:35
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
� All• 1�����1 �'
Page 17 of 20
3004.1.0.0
Aff- — Hduanced
Environmental Laboratories, Inc.
QUALITY CONTROL DATA
Workorder: J1501847 Hancock Bank Property
METHOD BLANK: 1696093
Blank Reporting
Parameter Units Result Limit Qualifiers
METALS
Mercury mg/L 0.000010 0.000010 U
Workorder: J1501847 Hancock Bank Property
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
QUALITY CONTROL DATA QUALIFIERS
QUALITY CONTROL PARAMETER QUALIFIERS
U The compound was analyzed for but not detected.
I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
J3 Lab QC Failure
J4 Estimated Result
0
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
o
h4'O c p�'y
U� z
Page 18 of 20
3004.1.0.0
AM flduanced
-= Environmental Laboratories, Inc.
Advanced Environmental Laboratories, Inc
6681 Southpoint Pkwy Jacksonville, FL 32216
Payments: P.O. Box 551580 Jacksonville, FL 32255-1580
Phone: (904)363-9350
Fax: (904)363-9354
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: J1501847 Hancock Bank Property
Analysis
Lab ID Sample ID Prep Method Prep Batch Analysis Method Batch
J1501847002
SB -4
SM 254OG
WCAj/1333
J1501847001
GW -1
SW -846 3010A
DGMj/1208
SW -846 6010
ICPj/1129
J1501847002
SB -4
SW -846 5035
MSVj/1206
SW -846 8260B
MSVj/1207
J1501847001
GW -1
SW -846 5030B
MSVj/1210
SW -846 8260B
MSVj/1211
J1501847002
SB -4
SW -846 3050B
DGMj/1211
SW -846 6010
ICPj/1133
J1501847002
SB -4
SW -846 3550B
EXTj/1252
SW -846 8270C
MSSj/1122
J1501847001
GW -1
SW -846 3510C
EXTj/1259
SW -846 8270C
MSSj/1120
J1501847002
SB -4
SW -846 7471A
DGMj/1216
SW -846 7471A
CVAj/1038
J1501847001
GW -1
SW -846 7470A
DGMj/1237
SW -846 7470A
CVAj/1041
Report ID: 357001 - 5175626
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Advanced Environmental Laboratories, Inc.
°Av
f Il �4
Page 19 of 20
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